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result(s) for
"Cardenas, Marco"
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Size Effects of Silver Nanoparticles and Magnetic Beads on Silver-Gold Galvanic Exchange in Aptamer-Based Electrochemical Assays
by
Alwarsh, Eman
,
Adrian, Daniel
,
Bui, Trang
in
Antibodies
,
Aptamers
,
Aptamers, Nucleotide - chemistry
2025
In this work, we investigated the influence of silver nanoparticle (AgNP) size (diameters of 20, 50, and 100 nm) and magnetic bead (MB) size (diameters from 100 to 4500 nm) on silver-gold galvanic exchange signal generation in magnetic electrochemical assays. Two conjugation strategies, including biotin-streptavidin interaction and a streptavidin-specific aptamer interaction, were compared to assess differences in binding chemistry and conjugation efficiency. Calibration studies showed that 50 nm diameter AgNPs provided the best sensitivity and galvanic exchange efficiency, yielding the lowest detection limits across both conjugation strategies. Larger AgNPs produced stronger signals but reached saturation rapidly, whereas smaller particles required higher concentrations to achieve equivalent silver content. Among MBs, 1000 nm beads consistently gave the highest galvanic exchange efficiency, offering sufficient surface area for AgNP loading while minimizing steric hindrance and electrode obstruction. These findings were confirmed by complementary electrochemical impedance spectroscopy, UV-Vis absorbance, and SEM imaging, which collectively demonstrated the strong influence of bead size on charge transfer resistance and conjugation efficiency. Overall, the combination of 50 nm AgNPs with 1000 nm MBs emerged as the optimal configuration, providing improved sensitivity and reproducibility. We believe these results offer valuable design guidelines for the development of next-generation aptamer-based electrochemical biosensors for biomarker detection.
Journal Article
Square Split-Ring Resonator as a Sensor for Detection of Nanoparticles in PVDF-Based Nanocomposites at Ultra-High Frequencies: MXenes and MoS2 Concentrations
by
Hernandez-Gonzalez, Emmanuel
,
Santos, Carlos Velasco
,
Mata-Lopez, Walter A.
in
Dielectric properties
,
Nanocomposites
,
Nanoparticles
2026
The performance of a printed square split-ring resonator as a sensor for quantifying nanoparticle concentrations in PVDF-based nanocomposites was evaluated at UHF frequencies. The sensing mechanism was based on the frequency response of parameter S21, observing the shift in the resonant frequency and a variation in S21 level, while samples were placed on the ring split and compared to the sensor without a sample. Experiments with samples of PVDF-based nanocomposites combined with different concentrations of both MoS2 and MXenes, ranging from 0.01% to 0.2%, were conducted. In general, considering both types of samples studied, it was observed that, as the concentration increases, S21 (dB) increases from −6.35 to −6 dB. At the same time, the resonance frequency in the S21 plot went from 500.4 to 498.25 MHz. Although the concentrations and their variations were relatively low, shifts in the resonance frequency of S21 were evident, demonstrating the ability of the sensor to detect low concentrations and variations of MoS2 and MXenes, being the detection of samples with higher concentrations feasible as future work, and concluding that the sensor had a relatively acceptable performance. In this study, MXenes were the concentrations that produced more noticeable shifts in the resonance frequency of S21. Likewise, characterizations based on SEM and TEM were performed to corroborate the ones at UHF frequencies.
Journal Article
A Z-Test-Based Evaluation of a Least Mean Square Filter for Noise Reduction
by
Pineda-Rico, Ulises
,
Cortés, Obed Pérez
,
Arce, Armando
in
Adaptation
,
adaptive
,
Adaptive filters
2025
This paper presents a comprehensive evaluation using a Z-test to assess the effectiveness of an adaptive Least Mean Squares (LMS) filter driven by the Steepest Descent Method (SDM). The study utilizes a male voice recording, captured in a controlled studio environment, to which persistent Gaussian noise was intentionally introduced, simulating real-world interference. All signal processing methods were implemented accordingly in MATLAB.version: 9.13.0 (R2022b), Natick, MA, USA: The MathWorks Inc.; 2022. The adaptive filter demonstrated a significant improvement of 20 dB in Signal-to-Noise Ratio (SNR) following the initial optimization of the filter parameter μ. To further assess the LMS filter’s performance, an empirical experiment was conducted with 30 young adults, aged between 20 and 30 years, who were tasked with qualitatively distinguishing between the clean and noise-corrupted signals (blind test). The quantitative analysis and statistical evaluation of the participants’ responses revealed that a significant majority, specifically 80%, were able to reliably identify the noise-affected and filtered signals. This outcome highlights the LMS filter’s potential—despite the slow convergence of the SDM—for enhancing signal clarity in noise-contaminated environments, thus validating its practical application in speech processing and noise reduction.
Journal Article
Recurrent Deep Learning for Beam Pattern Synthesis in Optimized Antenna Arrays
by
Pineda-Rico, Ulises
,
Arce, Armando
,
Arce, Fernando
in
Algorithms
,
antenna arrays
,
antenna radiation patterns
2025
This work proposes and describes a deep learning-based approach utilizing recurrent neural networks (RNNs) for beam pattern synthesis considering uniform linear arrays. In this particular case, the deep neural network (DNN) learns from previously optimized radiation patterns as inputs and generates complex excitations as output. Beam patterns are optimized using a genetic algorithm during the training phase in order to reduce sidelobes and achieve high directivity. Idealized and test beam patterns are employed as inputs for the DNN, demonstrating their effectiveness in scenarios with high prediction complexity and closely spaced elements. Additionally, a comparative analysis is conducted among the three DNN architectures. Numerical experiments reveal improvements in performance when using the long short-term memory network (LSTM) compared to fully connected and convolutional neural networks.
Journal Article
Superimposed Training Combined Approach for a Reduced Phase of Spectrum Sensing in Cognitive Radio
by
Pineda-Rico, Ulises
,
Lopez-Lopez, Lizeth
,
Arce, Armando
in
Acoustics
,
Algorithms
,
cognitive radio
2019
This paper presents an approach to exploit the superimposed training (ST)-based primary users’ (PUs) transmissions in the context of spectrum sensing for cognitive radio. In the low signal-to-noise ratio (SNR), the proposed scheme splits the spectrum sensing phase into two sample processing periods, allowing a secondary user (SU) to carry out a training sequence synchronization (with a small probability of error) before the implementation of a robust spectrum sensing algorithm that enhances the detection, based on the deterministic signal components embedded in the ST PU’s signals along with the unknown data signal. The overall sensing performance is improved using a reasonable number of samples to achieve a high probability of detection, resulting in a reduced spectrum sensing duration. Furthermore, a low computational complexity version of the proposed ST combined approach for a reduced phase (SCAR-Phase) of spectrum sensing is presented, which attains the same detection performance with a smaller number of real operations in the low SNR. In the practical consideration of imperfect training sequence synchronizations, the results show the advantages of exploiting the ST sequence to perform spectrum sensing, thus quantifying the significant improvement in detection performance and the maximum SU’s achievable throughput.
Journal Article
Evaluation of the Microwave Absorption Properties of Solid Dehydrated and Powdered Agricultural Waste at X ‐Band Frequencies
by
Hernandez-Gonzalez, Emmanuel
,
Villanueva-Maldonado, Juvenal
,
Maciel-Barboza, Fermin Marcelo
in
Agricultural pollution
,
Agricultural wastes
,
Agriculture
2024
In this article, a comparison of the absorption properties of 7 common agricultural waste materials from the state of Colima in Mexico is performed. The study carried out at X ‐band frequencies finds that the highest absorption levels were mainly from 8 to 10.5 GHz. The experiment, based on a WR‐90 waveguide with samples inserted in holders in the middle of it, shows that papaya peel and lemon peel had the highest absorption levels in the aforementioned frequency range. This study is relevant because of the vast amount of agricultural waste generated in such state of Mexico, that can be used as absorbers in the microwave regime, and not managed as garbage. In this work, the feasibility of using these eco‐friendly and nontoxic materials as microwave absorbers instead of typical commercial synthetic materials is evaluated.
Journal Article
Design of an Ultrawideband Circularly Polarized Printed Crossed-Dipole Antenna Based on Genetic Algorithms for S-Band CubeSat Applications
by
Villanueva-Maldonado, Juvenal
,
Cardenas-Juarez, Marco
,
Flores-Troncoso, Jorge
in
Antennas
,
Backplanes
,
Bandwidths
2021
As in any satellite, onboard antennas for CubeSats are crucial to establish communication with ground stations or other satellites. According to its application, antennas must comply with standardized requirements related to size, bandwidth, operating frequency, polarization, and gain. This paper presents an ultrawideband circularly polarized two-layer crossed-dipole microstrip antenna for S-band CubeSat applications using genetic algorithms optimization tools included in the 3D electromagnetic simulation software Ansys HFSS. The antenna is constructed on a 10 × 10 cm Cuclad-250 substrate with a back copper flat plane, located at λ/4 at 2.25 GHz operating frequency. The backplane with the exact substrate dimensions improves gain and reduces inside satellite radiation. Measured bandwidth defined by S11 at a −10 dB was higher than 1835 MHz with S11 = −24.68 dB at the central frequency of 2.25 GHz, while measured VSWR at the same frequency was 1.124. At 2.25 GHz, the maximum measured gain and the minimum measured axial ratio in the broadside direction were found to be 6 dBi and 0.22 dB, respectively. There are antenna simulations and measurements, as long as its fabrication guarantees application requirements that make it ready for prespace testing.
Journal Article
A Second-Iteration Square Koch Fractal Slot Antenna for UHF Downlink Telemetry Applications in CubeSat Small Satellites
by
Arce, Armando
,
Briones, Edgar
,
Cardenas-Juarez, Marco
in
Acceptable noise levels
,
Antennas
,
Cubesat
2020
This article presents the design, fabrication, and measurement of a square Koch fractal slot antenna for UHF band using both the FR4-G10 and Cuclad 250 substrates. Conveniently, this 56.56 cm full-length antenna possesses a geometry that allows it to be incorporated into the standardized 10 cm × 10 cm faces of the CubeSats. Furthermore, it is shown that both selected substrates exhibit an acceptable performance at the frequency of interest despite the economic cost difference and relative permittivity. Hence, the commercial FR4-G10 antenna substrate can be preferred because of its low-cost and admissible performance at 458 MHz, which is a frequency in the UHF band that is commonly used for telemetry, tracking, and command downlinks of CubeSats. Measurements show that the proposed antenna exhibits a reflection coefficient of −16.53 dB, a bandwidth of 22.62 MHz at −10 dB, a VSWR of 1.3508, a normalized impedance of 0.794 − j0.173 at 50 Ω, and a directivity of 2.24 dBi. The contribution of this work consists in the use of a fractal geometry to construct a low-cost slot antenna working at UHF frequencies over the limited area of the CubeSat faces and in order to optimize the area for an eventual coexistence with solar cells.
Journal Article
Design and Optimization of a Coherent Beamforming Network for an Aperiodic Concentric Ring Array
by
Simón, Jorge
,
Pineda-Rico, Ulises
,
Stevens-Navarro, E.
in
Advantages
,
Antenna arrays
,
Antennas
2019
In this work, a flexible and reconfigurable feeding network design for a nonuniform aperture on circular concentric ring arrays is proposed and analyzed. The network subsystem delivers coherent in-phase outputs with a Gaussian-like amplitude distribution, in a modular and basic topology based on sets of alternated power combiners and dividers. A complete antenna system in a monobeam configuration with a coherent network based on grouped inputs (blocks) per ring for an aperiodic concentric ring array with beam scanning and beam shaping properties is synthesized and analyzed. Additionally, a comparative analysis based on nonuniform and uniform concentric ring arrays fed by the proposed coherent network configuration is conducted and assessed. The optimization of the aperiodic layout on the antenna aperture (radii and interelement antenna spacings) is done by the differential evolution algorithm. Numeric experimentation demonstrates the performance advantages and capabilities of the proposed coherent network configuration with a nonuniform aperture over its uniform counterpart, with an improvement in average equal to −8.7 dB of side lobe level and 3.9 dB of directivity. Furthermore, the numeric examples show a complexity reduction on the coherent feeding network configuration based on the number of control signal inputs compared with a conventional phased antenna array; in the proposed configuration, the main beam is steered and shaped with N-1 control feeding ports per ring in this antenna system.
Journal Article
Optimization of a Coherent Dual-Beam Array Feed Network for Aperiodic Concentric Ring Antennas
by
Pineda-Rico, Ulises
,
Castillo-Soria, Francisco R.
,
Arce, Armando
in
antenna synthesis
,
Antennas
,
aperiodic arrays
2021
A dual-beam coherent feeding system design approach with a non-uniform layout on a concentric ring array is described and synthesized. In this case, the feeding system is based on a reconfigurable topology composed of a set of alternated power dividers and combiners, providing coherent in-phase outputs. Thus, in this paper, a two-beam architecture based on a coherent feeding system formed by a set of intercalated input signals feeding each circular ring in a non-uniform antenna array with multi-beam shaping and steering features is analyzed. The task of optimizing the aperiodic layout on the shared aperture based on the radii of the circular rings is realized by the differential evolution method. Numerical experiments grounded in antenna synthesis validate the capabilities and improved performance of the proposed dual-beam configuration with a non-uniform layout in contrast with its uniform counterpart, with enhanced performance on average by up to −6.1 dB for sidelobe level and 3.5 dB for directivity. Additionally, the results show a significantly less complex two-beam feeding network in contrast with the case of a typical electronically scanned array—in this proposal, each direction of maximum radiation is conformed and scanned with approximately half of the control inputs.
Journal Article