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15 result(s) for "Litovchenko, Igor"
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The Effect of Structural States on the Microstructure and Mechanical Properties of Low-Activation Austenitic Steel After Long-Term Thermal Exposure at 700 °C
The microstructure of a high-manganese low-activation austenitic steel after aging for 500 and 1000 h at 700 °C was investigated using transmission and scanning electron microscopy. Two structural states were examined: cold rolling (CR) and high-temperature thermomechanical treatment (HTMT). After CR, aging leads to the precipitation of dispersed M23C6 carbides (M = Cr, W), primarily along grain and deformation twin boundaries. After HTMT, these particles are mainly localized at grain and low-angle boundaries. With increasing aging time, both the size and volume fraction of the particles increase. In both states, the microtwin and substructure are partially retained after aging. Local regions corresponding to the early stages of recrystallization were identified after both treatments. These regions were associated with intense decomposition of the supersaturated solid solution and the coarsening of carbide particles. The mechanical properties were evaluated by tensile testing at 20, 650, and 700 °C. Aging reduced average ductility after both treatments and at all test temperatures, with this trend persisting with increasing aging time. After CR and aging, a significant scatter in elongation to failure was observed, with minimum values of ≈2–3%. This behavior is attributed to the high density of plate-like M23C6 carbides at grain and microtwin boundaries. Microcrack formation and intercrystalline fracture features were observed, directly linked to the high density of boundary carbides. These effects were less pronounced in the HTMT condition after aging. In this paper, strategies for suppressing carbide precipitation in high-manganese low-activation austenitic steels via chemical composition and thermomechanical processing optimization are discussed.
Structural Transformations and Mechanical Properties of Metastable Austenitic Steel under High Temperature Thermomechanical Treatment
The effect of high-temperature thermomechanical treatment on the structural transformations and mechanical properties of metastable austenitic steel of the AISI 321 type is investigated. The features of the grain and defect microstructure of steel were studied by scanning electron microscopy with electron back-scatter diffraction (SEM EBSD) and transmission electron microscopy (TEM). It is shown that in the initial state after solution treatment the average grain size is 18 μm. A high (≈50%) fraction of twin boundaries (annealing twins) was found. In the course of hot (with heating up to 1100 °C) plastic deformation by rolling to moderate strain (e = 1.6, where e is true strain) the grain structure undergoes fragmentation, which gives rise to grain refining (the average grain size is 8 μm). Partial recovery and recrystallization also occur. The fraction of low-angle misorientation boundaries increases up to ≈46%, and that of twin boundaries decreases to ≈25%, compared to the initial state. The yield strength after this treatment reaches up to 477 MPa with elongation-to-failure of 26%. The combination of plastic deformation with heating up to 1100 °C (e = 0.8) and subsequent deformation with heating up to 600 °C (e = 0.7) reduces the average grain size to 1.4 μm and forms submicrocrystalline fragments. The fraction of low-angle misorientation boundaries is ≈60%, and that of twin boundaries is ≈3%. The structural states formed after this treatment provide an increase in the strength properties of steel (yield strength reaches up to 677 MPa) with ductility values of 12%. The mechanisms of plastic deformation and strengthening of metastable austenitic steel under the above high-temperature thermomechanical treatments are discussed.
Microstructure Features and Mechanical Properties of Modified Low-Activation Austenitic Steel in the Temperature Range of 20 to 750 °C
A new low-activation austenitic steel with a modified composition and high austenite stability is proposed. The features of its microstructure after solution treatment (ST) and cold rolling (CR) are studied. The mechanical properties and features of the fracture behavior of this steel under tensile tests in the temperature range of 20–750 °C are discussed. After ST, an austenitic structure with stacking faults and dispersed carbide particles of the MC and M23C6 types is observed in the steel. After CR, the grains are refined, and the average grain size decreases from 41.4 µm (after ST) to 33.9 µm. High-density microtwin packets form in the material, and the dislocation density increases relative to that after ST. As the test temperature increases from 20 to 750 °C, the yield strength of the steel decreases by approximately two times, from ≈300 to 150 MPa (for ST) and from ≈700 to 370 MPa (for CR). In the studied temperature range, the steel demonstrates up to 2.6 times higher values of elongation to failure, ≈40–80% (for ST) and ≈13–27% (for CR), compared to steels of similar compositions and lower manganese content. Mechanical twinning contributes to the high steel ductility up to 300 °C. Signs of discontinuous flow in the tensile curves after ST in the temperature range of 500–600 °C and a decrease in the elongation to failure in the close temperature range indicate dynamic strain aging (DSA). Steel fracture after tension at all test temperatures mainly occurs via a ductile dimple transcrystalline mechanism with elements of ductile intercrystalline fracture. It is shown that cracks nucleate on clusters of dispersed second-phase particles. The mechanisms of plastic deformation, fracture, and strengthening of the proposed modified low-activation austenitic steel are discussed.
The Microstructure and Mechanical Properties of Ferritic-Martensitic Steel EP-823 after High-Temperature Thermomechanical Treatment
The effect of high-temperature thermomechanical treatment (HTMT) with plastic deformation by rolling in austenitic region on the microstructure and mechanical properties of 12% chromium ferritic-martensitic steel EP-823 is investigated. The features of the grain and defect microstructure of steel are studied by Scanning Electron Microscopy with Electron Back-Scatter Diffraction (SEM EBSD) and Transmission Electron Microscopy (TEM). It is shown that HTMT leads to the formation of pancake structure with grains extended in the rolling direction and flattened in the rolling plane. The average sizes of martensitic packets and ferrite grains are approximately 1.5–2 times smaller compared to the corresponding values after traditional heat treatment (THT, which consists of normalization and tempering). The maximum grain size in the section parallel to the rolling plane increases up to more than 80 µm. HTMT leads to the formation of new sub-boundaries and a higher dislocation density. The fraction of low-angle misorientation boundaries reaches up to ≈68%, which exceeds the corresponding value after HTMT (55%). HTMT does not practically affect the carbide subsystem of steel. The mechanical properties are investigated by tensile tests in the temperature range 20–700 °C. It is shown that the values of the yield strength in this temperature range after HTMT increase relative to the corresponding values after THT. As a result of HTMT, the elongation decreases. A significant decrease is observed in the area of dynamic strain aging (DSA). The mechanisms of plastic deformation and strengthening of ferritic-martensitic steel under the high-temperature thermomechanical treatments are also discussed.
Effect of Multistage High Temperature Thermomechanical Treatment on the Microstructure and Mechanical Properties of Austenitic Reactor Steel
The deformation microstructures formed by novel multistage high-temperature thermomechanical treatment (HTMT) and their effect on the mechanical properties of austenitic reactor steel are investigated. It is shown that HTMT with plastic deformation at the temperature decreasing in each stage (1100, 900, and 600 °C with a total strain degree of e = 2) is an effective method for refining the grain structure and increasing the strength of the reactor steel. The structural features of grains, grain boundaries and defective substructure of the steel are studied in two sections (in planes perpendicular to the transverse direction and perpendicular to the normal direction) by Scanning Electron Microscopy with Electron Back-Scatter Diffraction (SEM EBSD) and Transmission Electron Microscopy (TEM). After the multistage HTMT, a fragmented structure is formed with grains elongated along the rolling direction and flattened in the rolling plane. The average grain size decreases from 19.3 µm (for the state after solution treatment) to 1.8 µm. A high density of low-angle boundaries (up to ≈ 80%) is found inside deformed grains. An additional cold deformation (e = 0.3) after the multistage HTMT promotes mechanical twinning within fragmented grains and subgrains. The resulting structural states provide high strength properties of steel: the yield strength increases up to 910 MPa (at 20 °C) and up to 580 MPa (at 650 °C), which is 4.6 and 6.1 times higher than that in the state after solution treatment (ST), respectively. The formation of deformed substructure and the influence of dynamic strain aging at an elevated tensile temperature on the mechanical properties of the steel are discussed. Based on the results obtained, the multistage HTMT used in this study can be applied for increasing the strength of austenitic steels.
The Microstructure and Tensile Properties of New High-Manganese Low-Activation Austenitic Steel
Using X-ray diffraction, scanning and transmission electron microscopy, the microstructure of a new low-activation chromium-manganese austenitic steel with a high content of manganese and strong carbide-forming elements is studied. Its structure, dislocation character and particle composition are detailed. The processes taking place in the steel under cold-rolling deformation are described. It is shown that the mechanical properties of the new high-manganese steel revealed by testing at 20 and 650 °C are comparable with those of well-known analogs or exceed them. Relying on the structural studies, this is attributed to the dispersion and substructural strengthening. Better plastic properties of the steel are associated with the twinning-induced plasticity effect. It is shown that the steel fracture after tension at the test temperatures is mainly ductile dimple transcrystalline with the elements of ductile intercrystalline fracture (at 20 °C), while at 650 °C the signs of the latter disappear. The low-activation chromium-manganese austenitic steels characterized by increased austenite stability are thought to be promising structural materials for nuclear power engineering.
THE STUDY OF THE BAKING OVENS BY COMPUTER SIMULATION
Configuring ovens for baking bread is a complex scientific and industrial problems. Find the best modes of operation allows computer simulation of aerodynamic and thermal processes in the heating ducts and the baking chamber. Shows an example of a motion study of heating gases in areas of attention, shows the typical problems and methods their solutions.
The Microstructure, Tensile and Impact Properties of Low-Activation Ferritic-Martensitic Steel EK-181 after High-Temperature Thermomechanical Treatment
In this work, we study the effect of high-temperature thermomechanical treatment (HTMT) with deformation in the austenite region on the microstructure, tensile properties, impact toughness, and fracture features of advanced low-activation 12% chromium ferritic-martensitic reactor steel EK-181. HTMT more significantly modifies the steel structural-phase state than the traditional heat treatment (THT). As a result of HTMT, the hierarchically organized structure of steel is refined. The forming grains and subgrains are elongated in the rolling direction and flattened in the rolling plane (so-called pancake structure) and have a high density of dislocations pinned by stable nanosized particles of the MX type. This microstructure provides a simultaneous increase, relative to THT, in the yield strength and impact toughness of steel EK-181 and does not practically change its ductile-brittle transition temperature. The most important reasons for the increase in impact toughness are a decrease in the effective grain size of steel (martensite blocks and ferrite grains) and the appearance of a crack-arrester type delamination perpendicular to the main crack propagation direction. This causes branching of the main crack and an increase in the absorbed impact energy.
The Cold-Brittleness Regularities of Low-Activation Ferritic-Martensitic Steel EK-181
The behavior of the EK-181 low-activation ferritic-martensitic reactor steel (Fe–12Cr–2W–V–Ta–B) in the states with different levels of strength and plastic properties after traditional heat treatment (THT) and after high-temperature thermomechanical treatment (HTMT) in the temperature range from −196 to 25 °C, including the range of its cold brittleness (ductile–brittle transition temperature, DBTT) is studied. The investigations are carried out using non-destructive acoustic methods (internal friction, elasticity) and transmission and scanning electron microscopy methods. It is found that the curves of temperature dependence of internal friction (the vibration decrement) of EK-181 steel after THT and HTMT are similar to those of its impact strength. Below the ductile–brittle transition temperature, it is characterized by a low level of dislocation internal friction. The temperature dependence curves of the steel elastic modulus increase monotonically with the decreasing temperature. In this case, the value of Young’s modulus is structure-sensitive. A modification of the microstructure of EK-181 steel as a result of HTMT causes its elastic modulus to increase, compared to that after THT, over the entire temperature range under study. The electron microscopic studies of the steel microstructure evolution near the fracture surface of the impact samples (in the region of dynamic crack propagation) in the temperature range from −196 to 100 °C reveal the traces of plastic deformation (increased dislocation density, fragmentation of the martensitic structure) at all of the temperatures under study, including those below the cold brittleness threshold of EK-181 steel.
Current incidence of professional burnout among Ukrainian oncologists in Kharkiv
Severe acute respiratory syndrome coronavirus 2 (SARS-CoV-2) pandemic and the military conflicts in Ukraine suggest that workrelated stressors increased during these crises increases work-related stress reactions. Burnout as a long-term consequence of insufficiently compensated for workloads. The regional prevalence of burnout is particularly high among oncologists. The aim of this study was to assess the current risk of burnout within this group of physicians and to examine gender differences through gender-based analysis. Thirtyseven oncologists (17 men and 20 women aged 46.5±13.6 years [range 26-74 years]) in Kharkiv, Ukraine, participated. The (MBI-GS) questionnaire was used to determine the extent of occupational. Gender, age, and work experience had no effect on the following results. Women demonstrated higher scores in emotional exhaustion and personal accomplishment of the MBI than men. In contrast, men offered higher cynicism scores. The MBI total score was also higher for the male oncologists. Only 1 person of the total sample had risk of burnout. The results showed a high prevalence of burnout symptoms among Ukrainian oncologists without gender differences. From occupational health perspective behavioral and behavior-preventive measures are needed for clinics and oncologists to counteract the burnout symptoms, e.g. exhaustion or cyniscism. Further studies are needed here to examine the effectiveness of these measures. Int J Occup Med Environ Health. 2023;36(6):717-3.