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The current paper studies the influence of geometrical parameters of the fused deposition modeling (FDM)—fused filament fabrication (FFF) 3D printing process on printed part strength for open source desktop 3D printers and the most popular material used for that purpose—i.e., polylactic acid (PLA). The study was conducted using a set of different nozzles (0.4, 0.6, and 0.8 mm) and a range of layer heights from the minimum to maximum physical limits of the machine. To assess print strength, a novel assessment method is proposed. A tubular sample is loaded in the weakest direction (across layers) in a three-point bending fixture. Mesostructure evaluation through scanning electronic microscopy (SEM) scans of the samples was used to explain the obtained results. We detected a significant influence of geometric process parameters on sample mesostructure, and consequently, on sample strength.

Purpose This paper aims to investigate how the user-controlled parameters of the fused filament fabrication three-dimensional printing process define temperature conditions on the boundary between layers of the part being fabricated and how these conditions influence the structure and strength of the polylactic acid part. Design/methodology/approach Fracture load in a three-point bending test and calculated related stress were used as a measure. The samples were printed with the long side along the z-axis, thus, in the bend tests, the maximum stress occurred orthogonally to the layers. Temperature distribution on the sample surface during printing was monitored with a thermal imager. Sample mesostructure was analyzed using scanning electron microscopy. The influence of the extrusion temperature, the intensity of part cooling, the printing speed and the time between printing individual layers were considered. Findings It is shown that the optimization of the process parameters responsible for temperature conditions makes it possible to approximate the strength of the interlayer cohesion to the bulk material strength. Originality/value The novelty of the study consists in the generalization of the outcomes. All the parameters varied can be expressed through two factors, namely, the temperature of the previous layer and the extrusion efficiency, determining the ratio of the amount of extruded plastic to the calculated. A regression model was proposed that describes the effect of the two factors on the printed part strength. Along with interlayer bonding strength, these two factors determine the formation of the part mesostructure (the geometry of the boundaries between individual threads).

This paper studies the effect of the laser melting process (LMP) on the microstructure and hardness of a new modified AlCuMgMn alloy with zirconium (Zr) and Yttrium (Y) elements. Homogenized (480 °C/8 h) alloys were laser-surface-treated at room temperature and a heating platform with in situ heating conditions was used in order to control the formed microstructure by decreasing the solidification rate in the laser-melted zone (LMZ). Modifying the AlCuMgMn alloy with 0.4 wt% Zr and 0.6 wt% Y led to a decrease in grain size by 25% with a uniform grain size distribution in the as-cast state due to the formation of Al3(Y, Zr). The homogenization dissolved the nonequilibrium intermetallic phases into the (Al) matrix and spheroidized and fragmentized the equilibrium phase’s particles, which led to the solidification of the crack-free LM zone with a nonuniform grain structure. The microstructure in the LMZ was improved by using the in situ heating approach, which decreased the temperature gradient between the BM and the melt pool. Two different microstructures were observed: ultrafine grains at the boundaries of the melted pool due to the extremely high concentration of optimally sized Al3(Y, Zr) and fine equiaxed grains at the center of the LMZ. The combination of the presence of ZrY and applying a heating platform during the LMP increased the hardness of the LMZ by 1.14 times more than the hardness of the LMZ of the cast AlCuMgMn alloy.

AlZnMgCu, the high-strength aluminum alloy, is unsuitable for laser melting applications due to its high hot cracking sensitivity and large solidification temperature range. Adapting this alloy for laser melting processing is a high-demand research issue for extending its use. Thus, this paper investigates the effect of adding 4%Si, 4%Si-Sc+Zr, 4%Si-Ti+B, and homogenization annealing on the laser melting process (LMP) of AlZnMgCu alloy. Homogenization annealing at 500 °C for 6.5 h was selected to dissolve most of the low melting temperature phases into the grain matrix and perform stable alloys for the LMP. The pulsed laser melting process (PLM) was performed on the as-casted and the homogenized samples. The microstructures of the as-casted, the homogenized alloys, and after the LMP were evaluated. In addition, the hardness of the base metal (BM) and laser melted zone (LMZ) were measured. The results revealed that the microstructure was enhanced and refined in the as-cast state by adding the modifiers due to the increasing nucleation potency of solidification sites and the formation of primary Al3(Ti, Zr, Sc) phases. The average grain size was decreased by 15.6 times when adding 4%Si + 0.4%Zr + 0.29%Sc, while it decreased by 10.2 times when adding 4%Si + 1%Ti + 0.2%B. The LMZ of the as-casted samples exhibited a non-uniform distribution of the grains and the elements after the LMP. This was attributed to the evaporation of Zn, Mg during the high laser power process besides the non-uniform distribution of elements and phases in samples during casting. After the laser treating of the homogenized samples with 4%Si-Sc + Zr, uniform columnar grains were formed in the direction of the laser. The presence of Ti and B changed the crystallization nature, resulting in the LMZ with very fine and equiaxed grains due to forming many nucleation centers during solidification. The hardness values have positively increased due to Si addition and adding a combination of Ti + B and Sc + Zr. The maximum hardness was 153.9 ± 5 HV achieved in the LMZ of the homogenized samples of 4%Si + 1%Ti + 0.2%B.

The mechanical properties and microstructure of as-cast and homogenized AA7075 were investigated. This alloy was modified by adding transition elements 0.3%Sc + 0.5%Zr, 1%Ti + 0.2%B, and 1%Fe + 1%Ni for use in additive manufacturing applications. After adding Ti + B and Sc + Zr, the structure became uniform and finer with the formation of the Al3(Sc, Zr) and TiB2 phases. Coarse structures were obtained with the formation of an extremely unfavorable morphology, close to a needle-like structure when Fe + Ni was added. The mechanical properties of the modified alloys were increased compared to those of the standard alloy, where the best ultimate tensile strength (UTS) and yield strength (YS) were obtained in the AA7075-TiB alloy compared to the standard alloy in as-cast and homogenized conditions, and the highest hardness value was provided by Fe + Ni additives. The effect of the laser melting process on the microstructure and mechanical properties was investigated. Single laser melts were performed on these alloys using 330 V and a scanning speed of 8 mm/s. During the laser melting, the liquation of the alloying elements occurred due to non-equilibrium solidification. A change in the microstructures was observed within the melt zone and heat-affected zone (HAZ). The hardness of the laser-melted zone (LMZ) after adding the modification elements was increased in comparison with that of the standard alloy. Corrosion testing was performed using a solution of 100 mL distilled water, 3.1 g NaCl, and 1 mL HCl over 5, 10, and 30 min and 1 and 2 h. The corrosion resistance of the alloy modified with FeNi was low because of the non-uniform elemental distribution along the LMZ, but in the case of modification with ScZr and TiB, the corrosion resistance was better compared to that of the standard alloy.

The hot deformation behaviour of an Al4.5Zn4.5Mg1Cu0.12Zr based alloy with 0.05, 0.1 and 0.15% Sc was investigated at temperatures between 300–450 °C and a strain rate of 0.1–15 s−1. The materials constants of a flow stress model based on the Zener-Hollomon parameter were determined (AARE was 5.8%). Three-dimensional processing maps were established by combining power dissipation efficiency and flow stability diagrams. Based on processing maps analysis and microstructures investigations, the optimal deformation parameters were determined as a temperature range of 350–400 °C and strain rates of 0.1–1 s−1 for the alloys with 0.05% and 0.1% Sc, and 0.1 s−1 for the alloy with 0.15% Sc.

The current study aims to evaluate the possibilities to increase part strength by optimizing the Fused Filament Fabrication (FFF) process parameters. Five different CAD models of parts with the same coupling dimensions but of different shape inherited from a recent study were converted into test samples with Ultimaker 2 3D printer. The main measure of success was the sample strength, defined as the load at which the first crack in the stressed area of the part appeared. Three different modifications to the FFF process with verified positive effect on interlayer bonding were applied. The first modification included raising the extrusion temperature and disabling printed part cooling. The second modification consisted of reduction in the layer thickness. The third modification combined the effects of the first and the second ones. For four out of five shapes tested the applied process modifications resulted in significant strengthening of the part. The shape that exhibited the best results was subject to further research by creating special printing mode. The mode included fine-tuning of three technological parameters on different stages of the part fabrication. As a result it was possible to increase the part strength by 108% only by tuning printing parameters of the best shape designed with increasing its weight by 8%.

The ability to form closed cavities inside the part printed is an important feature of Fused Filament Fabrication technology. A typical part consists of a dense shell bearing the primary load, filled with low-density plastic scaffold (infill). Such a constitution of the part provides in most cases appropriate strength and low weight. However, if the printed part shape includes horizontal (orthogonal to printer’s Z axis) flat surfaces other than its top and bottom surface, then the shell of the part becomes interrupted, which may lead to drastic drop in the ability of the part to withstand loads. In the current study, a representative sample of a part with interrupted shell and testing apparatus is developed. Influence of shell and base thicknesses, as well as influence of the infill density on the part strength, are studied. Different approaches to the sample shape modification were applied and tested. The part shape optimization made with respect to peculiarities of Fused Filament Fabrication technology resulted in increment of the force, required to fracture the part from 483 to 1096 N and in decreased part mass from 36.9 to 30.2 g.

High-strength crystalline/amorphous composites materials based on (Ti-Ni)-(Cu-Zr) system were developed. The optimal concentrations of additional alloying elements Al, Fe, and Cr were obtained. Structural investigations were carried out using X-ray diffraction equipment (XRD) and scanning electron microscope (SEM) with an energy-dispersive X-ray module (EDX). It was found that additives of aluminum and chromium up to 5 at% dissolve well into the solid matrix solution of the NiTi phase. At a concentration of 5 at%, the precipitation of the unfavorable NiTi2 phase occurs, which, as a result, leads to a dramatic decrease in ductility. Iron dissolves very well in the solid solution of the matrix phase due to chemical affinity with nickel. The addition of iron does not cause the precipitation of the NiTi2 phase in the concentration range of 0–8 at%, but with an increase in concentration, this leads to a decrease in the mechanical properties of the alloy. The mechanical behavior of alloys was studied in compression test conditions on a universal testing machine. The developed alloys have a good combination of strength and ductility due to their dual-phase structure. It was shown that additional alloying elements lead to a complete suppression of the martensitic transformation in the alloys.

This research work aims at finding the optimum process parameters for the laser welding of AA7020 aluminium alloys. The use of 7xxx series alloys is limited because of weldability problems, such as hot cracking, porosity, and softening of the fusion zone despite its higher specific strength-to-weight ratio. AA7020 aluminium alloy was welded while varying the process parameters so as to obtain optimal welding efficiency. The welded samples were analysed to reveal the microstructure, defects, and mechanical properties of the welded zone. The samples were prepared from a plate of AA7020, which was hot rolled at a temperature of 470 °С to a thickness of 1 mm. The welding was carried out at an overlap of 0.25 mm, duration of 14 ms and argon shield gas flow rate of 15 L/min. Process parameters, such as peak power, welding speed, and pulse shaping, were varied. The samples were welded with Al-5Ti-B and Al-5Mg as filler metals. The welding speed, peak power, and pulse shaping have a great influence on the weldability and hot cracking susceptibility of the aluminium alloy. Al-5Ti-B improves the microstructure and ultimate tensile strength of AA7020 aluminium alloy.