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Layer-by-layer deposition of materials to manufacture parts—better known as three-dimensional (3D) printing or additive manufacturing—has been flourishing as a fabrication process in the past several years and now can create complex geometries for use as models, assembly fixtures, and production molds. Increasing interest has focused on the use of this technology for direct manufacturing of production parts; however, it remains generally limited to single-material fabrication, which can limit the end-use functionality of the fabricated structures. The next generation of 3D printing will entail not only the integration of dissimilar materials but the embedding of active components in order to deliver functionality that was not possible previously. Examples could include arbitrarily shaped electronics with integrated microfluidic thermal management and intelligent prostheses custom-fit to the anatomy of a specific patient. We review the state of the art in multiprocess (or hybrid) 3D printing, in which complementary processes, both novel and traditional, are combined to advance the future of manufacturing.

While NASA explores the power of 3D printing in the development of the next generation space exploration vehicle, a CubeSat Trailblazer was launched in November 2013 that integrated 3D-printed structures with embedded electronics. Space provides a harsh environment necessary to demonstrate the durability of 3D-printed devices with radiation, extreme thermal cycling, and low pressure—all assaulting the structure at the atomic to macroscales. Consequently, devices that are operational in orbit can be relied upon in many terrestrial environments—including many defense and biomedical applications. The 3D-printed CubeSat module (a subsystem occupying approximately 10 % of the total volume offered by the 10 × 10 × 10-cm CubeSat enclosure) has a substrate that fits specifically into the available volume—exploiting 3D printing to provide volumetric efficiency. Based on the best fabrication technology at the time for 3D-printed electronics, stereolithography (SL), a vat photopolymerization technology, was used to fabricate the dielectric structure, while conductive inks were dispensed in channels to provide the electrical interconnect between components. In spite of the structure passing qualification—including temperature cycling, shock and vibration, and outgas testing—the photocurable materials used in SL do not provide the level of durability required for long-term functionality. Moreover, the conductive inks with low-temperature curing capabilities as required by the SL substrate material are widely known to provide suboptimal performance in terms of conductivity. To address these challenges in future 3D-printed electronics, a next generation machine is under development and being referred to as the multi 3D system, which denotes the use of multiple technologies to produce 3D, multi-material, multifunctional devices. Based on an extrusion process necessary to replace photocurable polymers with thermoplastics, a material extrusion system based on fused deposition modeling (FDM) technology has been developed that integrates other technologies to compensate for FDM’s deficiencies in surface finish, minimum dimensional feature size, and porosity. Additionally, to minimize the use of conductive inks, a novel thermal embedding technology submerges copper wires into the thermoplastic dielectric structures during FDM process interruptions—providing high performance, robust interconnect, and ground planes—and serendipitously improving the mechanical properties of the structure. This paper compares and contrasts stereolithography used for 3D-printed electronics with the FDM-based system through experimental results and demonstrates an automated FDM-based process for producing features not achievable with FDM alone. In addition to the possibility of using direct write for electronic circuitry, the novel fabrication uses thermoplastics and copper wires that offer a substantial improvement in terms of performance and durability of 3D-printed electronics.

Purpose - The purpose of this paper is to present a hybrid manufacturing system that integrates stereolithography (SL) and direct print (DP) technologies to fabricate three-dimensional (3D) structures with embedded electronic circuits. A detailed process was developed that enables fabrication of monolithic 3D packages with electronics without removal from the hybrid SL DP machine during the process. Successful devices are demonstrated consisting of simple 555 timer circuits designed and fabricated in 2D (single layer of routing) and 3D (multiple layers of routing and component placement).Design methodology approach - A hybrid SL DP system was designed and developed using a 3D Systems SL 250 50 machine and an nScrypt micro-dispensing pump integrated within the SL machine through orthogonally-aligned linear translation stages. A corresponding manufacturing process was also developed using this system to fabricate 2D and 3D monolithic structures with embedded electronic circuits. The process involved part design, process planning, integrated manufacturing (including multiple starts and stops of both SL and DP and multiple intermediate processes), and post-processing. SL provided substrate mechanical structure manufacturing while interconnections were achieved using DP of conductive inks. Simple functional demonstrations involving 2D and 3D circuit designs were accomplished.Findings - The 3D micro-dispensing DP system provided control over conductive trace deposition and combined with the manufacturing flexibility of the SL machine enabled the fabrication of monolithic 3D electronic structures. To fabricate a 3D electronic device within the hybrid SL DP machine, a process was developed that required multiple starts and stops of the SL process, removal of uncured resin from the SL substrate, insertion of active and passive electronic components, and DP and laser curing of the conductive traces. Using this process, the hybrid SL DP technology was capable of successfully fabricating, without removal from the machine during fabrication, functional 2D and 3D 555 timer circuits packaged within SL substrates.Research limitations implications - Results indicated that fabrication of 3D embedded electronic systems is possible using the hybrid SL DP machine. A complete manufacturing process was developed to fabricate complex, monolithic 3D structures with electronics in a single set-up, advancing the capabilities of additive manufacturing (AM) technologies. Although the process does not require removal of the structure from the machine during fabrication, many of the current sub-processes are manual. As a result, further research and development on automation and optimization of many of the sub-processes are required to enhance the overall manufacturing process.Practical implications - A new methodology is presented for manufacturing non-traditional electronic systems in arbitrary form, while achieving miniaturization and enabling rugged structure. Advanced applications are demonstrated using a semi-automated approach to SL DP integration. Opportunities exist to fully automate the hybrid SL DP machine and optimize the manufacturing process for enhancing the commercial appeal for fabricating complex systems.Originality value - This work broadly demonstrates what can be achieved by integrating multiple AM technologies together for fabricating unique devices and more specifically demonstrates a hybrid SL DP machine that can produce 3D monolithic structures with embedded electronics and printed interconnects.

One of the most common materials utilized by material extrusion 3D printing is acrylonitrile butadiene styrene (ABS). The work presented in this research explored the effect of the addition of reinforcing materials on the mechanical properties of ABS in an effort to create materials with enhanced physical properties. A comparison was made between pure ABS, two ABS matrix composites, and one ABS/elastomer blend with the purpose of characterizing the effect of additives on the mechanical properties. Tensile test results of specimens built in different orientations showed that ABS reinforced with 5% by weight TiO2 exhibited the highest ultimate tensile strength for specimens built in both horizontal and vertical directions with 32.2 and 18.4 MPa, respectively. The compounding of an elastomeric material with ABS improved the surface finish of parts as they were visibly smoother compared to those printed from the ABS baseline material, though there was an observable decrease in the ductility of tensile specimens. Analysis was performed on the fracture surface of the tensile specimens through the use of scanning electron microscopy. Fractography revealed different modes of failure related to the different additives. The effects of additives on the anisotropy associated with the mechanical properties of 3D-printed parts were also analyzed.[PUBLICATION ABSTRACT]

Purpose - The purpose of this paper is to investigate the effects of aging, pre-conditioning, and build orientation on the mechanical properties of test samples fabricated using stereolithography (SL) and a commercially available resin.Design methodology approach - American Society for Testing and Materials (ASTM) Standard D638 Type I specimens were manufactured in a Viper si2 SL system using WaterShed™ 11120 resin. The specimens were manufactured in two different build setups, designed to fit batches of 18 or 24 specimens with different build orientations. The specimens were randomly tested in tension, and a design of experiments (DOE) was used to determine the effect of aging (4, 30 or 120 days), pre-conditioning (ambient, desiccant, or ASTM recommended conditioning), and build orientation (flat, on an edge, or vertical) on the ultimate tensile stress (UTS) and elastic modulus (E) of SL fabricated samples. Additionally, the fractured samples were imaged using scanning electron microscopy (SEM) to characterize the fractured surfaces.Findings - Results showed that aging, pre-conditioning, and build orientation each had an effect on the mechanical properties of the SL samples. In general, the samples aged at the shortest time frame (4 days) and the samples preconditioned according to ASTM recommendations had the lowest values of UTS. Regarding the effect of build orientation, the specimens built flat (with layers oriented along the thickness of the sample) had the lowest UTS and E values and the mechanical properties were statistically different from those built vertically or on an edge. The specimens built in the vertical orientation (with layers oriented along the length of the sample) had the highest values of UTS and E, yet the mechanical properties of the samples built on an edge (with layers oriented along the width of the sample) were not statistically different from the samples built vertically. SEM images of the fractured specimens showed fracture surfaces typical of polymers with a mirror zone and changes in surface texture from smooth to coarse.Research limitations implications - The research was limited to a single commercially available resin. Through a statistical DOE approach, statistically significant differences in mechanical properties of SL fabricated samples were found as functions of aging, pre-conditioning, and build orientation. These results can assist the ASTM F42 Committee with developing test standards specific to SL and the additive manufacturing community.Originality value - The statistical analyses presented here can help identify and classify the effects of fabrication, storage, and conditioning parameters on mechanical properties for SL fabricated parts. Understanding how the mechanical properties of SL resins are affected by different parameters can help improve the use of SL for a variety of applications including direct manufacturing of end-use products.

Material extrusion 3D printing (ME3DP) based on fused deposition modeling (FDM) technology is currently the most commonly used additive manufacturing method. However, ME3DP suffers from a limitation of compatible materials and typically relies upon amorphous thermoplastics, such as acrylonitrile butadiene styrene (ABS). The work presented here demonstrates the development and implementation of binary and ternary polymeric blends for ME3DP. Multiple blends of acrylonitrile butadiene styrene (ABS), styrene ethylene butadiene styrene (SEBS), and ultrahigh molecular weight polyethylene (UHMWPE) were created through a twin screw compounding process to produce novel polymer blends compatible with ME3DP platforms. Mechanical testing and fractography were used to characterize the different physical properties of these new blends. Though the new blends possessed different physical properties, compatibility with ME3DP platforms was maintained. Also, a decrease in surface roughness of a standard test piece was observed for some blends as compared with ABS.

This paper presents some examples of knee and hip implant components containing porous structures and fabricated in monolithic forms utilizing electron beam melting (EBM). In addition, utilizing stiffness or relative stiffness versus relative density design plots for open-cellular structures (mesh and foam components) of Ti-6Al-4V and Co-29Cr-6Mo alloy fabricated by EBM, it is demonstrated that stiffness-compatible implants can be fabricated for optimal stress shielding for bone regimes as well as bone cell ingrowth. Implications for the fabrication of patient-specific, monolithic, multifunctional orthopaedic implants using EBM are described along with microstructures and mechanical properties characteristic of both Ti-6Al-4V and Co-29Cr-6Mo alloy prototypes, including both solid and open-cellular prototypes manufactured by additive manufacturing (AM) using EBM.

Purpose – The purpose of this paper is to investigate a build process variation for fused deposition modeling (FDM) in which contours and rasters (also referred to as internal fill patterns) are built using different layer thicknesses and road widths. In particular, the paper examines the effect of the build process variation on surface roughness, production times and mechanical properties. Additionally, a unique FDM process was developed that enabled the deposition of discrete multiple materials at different layers and regions within layers. Design/methodology/approach – A multi-material, multi-technology FDM system was developed and constructed to enable the production of parts using either discrete multi-materials or the build process variation (variable layer thickness and road width). Two legacy FDM machines were modified and installed onto a single manufacturing system to allow the strategic, spatially controlled thermoplastic deposition with multiple extrusion nozzles of multiple materials during the same build. This automated process was enabled by the use of a build platform attached to a pneumatic slide that moved the platform between the two FDM systems, an overall control system, a central PC and a custom-made program (FDMotion) and graphic user interface. The term multi-technology FDM system used here implies the two FDM systems and the integration of these systems into a single manufacturing environment using the movable platform and associated hardware and software. Future work will integrate additional technologies within this system. Parts produced using the build process variation utilized internal roads with 1,524 μm road width and 508 μm layer height, while the contours used 254 μm road width and 127 μm layer height. Measurements were performed and compared to standard FDM parts that included surface roughness of planes at different inclinations, tensile testing and fabrication times. Findings – Results showed that when compared to the standard FDM process, the parts produced using the build process variation exhibited the same tensile properties as determined by a student's t-test (p-values > 0.05, μ1-μ2 = 0, n = 5). Surface roughness measurements revealed that the process variation resulted in surface roughness (Ra) improvements of 55, 43, 44 and 38 per cent for respective planes inclined at 10, 15, 30 and 45° from vertical. In addition, for a 50.8 × 50.8 mm square section (25.4 mm tall), the build process variation required a minimum of 2.8 hours to build, while the standard FDM process required 6.0 hours constituting a 53 per cent reduction in build time. Finally, several manufacturing demonstrations were performed including the fabrication of a discrete PC-ABS sandwich structure containing tetragonal truss core elements. Originality/value – This paper demonstrates a build strategy that varies contour and raster widths and layer thicknesses for FDM that can be used to improve surface roughness – a characteristic that has historically been in need of improvement – and reduce fabrication time while retaining mechanical properties.

Material-extrusion three-dimensional (3D) printing has recently attracted much interest because of its process flexibility, rapid response to design alterations, and ability to create structures “on-the-go”. For this reason, 3D printing has possible applications in rapid creation of space-based devices, for example cube satellites (CubeSat). This work focused on fabrication and characterization of tungsten-doped polycarbonate polymer matrix composites specifically designed for x-ray radiation-shielding applications. The polycarbonate–tungsten polymer composite obtained intentionally utilizes low loading levels to provide x-ray shielding while limiting effects on other properties of the material, for example weight, electromagnetic functionality, and mechanical strength. The fabrication process, from tungsten functionalization to filament extrusion and material characterization, is described, including printability, determination of x-ray attenuation, tensile strength, impact resistance, and gigahertz permittivity, and failure analysis. The proposed materials are uniquely advantageous when implemented in 3D printed structures, because even a small volume fraction of tungsten has been shown to substantially alter the properties of the resulting composite.

An essentially fully acicular alpha-prime martensite within an equiaxed grain structure was produced in an Electron Beam Melting (EBM)-fabricated Ti-6Al-2Sn-4Zr-2Mo (Ti6242) alloy using two different Arcam EBM machines: An A2X system employing tungsten filament thermionic electron emission, and a Q20 system employing LaB6 thermionic electron emission. Post-process Hot Isostatic Pressing (HIP) treatment for 2 h at 850, 950, and 1050 °C resulted in grain refinement and equiaxed grain growth along with alpha-prime martensite decomposition to form an intragranular mixture of acicular martensite and alpha at 850 °C, and acicular alpha phase at 950 and 150 °C, often exhibiting a Widmanstätten (basketweave) structure. The corresponding tensile yield stress and ultimate tensile strength (UTS) associated with the grain growth and acicular alpha evolution decreased from ~1 and ~1.1 GPa, respectively, for the as-fabricated Ti6242 alloy to ~0.8 and 0.9 GPa, respectively, for HIP at 1050 °C. The optimum elongation of ~15–16% occurred for HIP at 850 °C; for both EBM systems. Because of the interactive role played by equiaxed grain growth and the intragrain, acicular alpha microstructures, the hardness varied only by ~7% between 41 and 38 HRC.