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The steady-state shear rheology of granular materials is investigated in slow quasistatic and inertial flows. The effect of gravity (thus the local pressure) and the often-neglected contact stiffness are the focus of this study. A series of particle simulations are performed on a weakly frictional granular assembly in a split-bottom geometry considering various magnitudes of gravity and contact stiffnesses. While traditionally the inertial number, i.e., the ratio of stress to strain-rate time scales, is used to describe the flow rheology, we report that a second dimensionless number, the ratio of softness and stress time scales, must also be included to characterize the bulk flow behavior. For slow, quasistatic flows, the density increases while the effective (macroscopic) friction decreases with increase in either particle softness or local pressure. This trend is added to the rheology and can be traced back to the anisotropy in the contact network, displaying a linear correlation between the effective friction coefficient and deviatoric fabric in the steady state. When the external rotation rate is increased towards the inertial regime, for a given gravity field and contact stiffness, the effective friction increases faster than linearly with the deviatoric fabric.

Using a combination of experimental techniques and discrete particle method simulations, we investigate the resonant behaviour of a dense, vibrated granular system. We demonstrate that a bed of particles driven by a vibrating plate may exhibit marked differences in its internal energy dependent on the specific frequency at which it is driven, even if the energy corresponding to the oscillations driving the system is held constant and the acceleration provided by the base remains consistently significantly higher than the gravitational acceleration, g. We show that these differences in the efficiency of energy transfer to the granular system can be explained by the existence of resonances between the bed's bulk motion and that of the oscillating plate driving the system. We systematically study the dependency of the observed resonant behaviour on the system's main, controllable parameters and, based on the results obtained, propose a simple empirical model capable of determining, for a given system, the points in parameter space for which optimal energy transfer may be achieved.

Mesoporous silicon and porous silicon/Ni nanocomposites have been investigated in this work employing light-dark surface photovoltage (SPV) transients to monitor the response of surface charge dynamics to illumination changes. The samples were prepared by anodization of a highly n-doped silicon wafer and a subsequent electrodepositing of Ni into the pores. The resulting pores were oriented towards the surface with an average pore diameter of 60 nm and the thickness of the porous layer of approximately 40 μm. SPV was performed on a bare porous silicon as well as on a Ni-filled porous silicon in vacuum and in different gaseous environments (O2, N2, Ar). A significant difference was observed between the ‘light-on’ and ‘light-off’ SPV transients obtained in vacuum and those observed in gaseous ambiences. Such behavior could be explained by the contribution to the charge exchange in gas environments from chemisorbed and physisorbed species at the semiconductor surface.PACS81.05.Rm; 73.20.-r; 75.50.-y; 82.45.Yz

We propose a simplified, theoretical approach of the evolution of liquid distribution during the convective drying of a granular packing. In the absence of gravity effects three regimes are distinguished according to the relative importance of surface evaporation, capillarity or evaporation from the interior of the sample. The evolution of the drying rate as a function of the saturation can be inferred from the characteristic velocities associated to each of these effects. We also carried out drying experiments of bead packings saturated with ethanol, at four different velocities of the boundary convection current, and with bead size ranging from 4.5 to 100 μm. The drying curves exhibit different regimes with a scaling as a function of particle radius and current velocity as predicted by the theory.

We investigate the macroscopic mechanical behaviour of wet polydisperse granular media. Capillary bonding between two grains of unequal diameters is described by a realistic force law implemented in a molecular-dynamics algorithm together with a protocol for the distribution of water in the bulk. Axial-compression tests are simulated for granular samples at different levels of water content, and compared to experiments performed in similar conditions. We find good agreement between numerical and experimental data in terms of the rupture strength as a function of water content. Our results show the importance of the distribution of water for the mechanical behaviour.

We report sets of precise and reproducible measurements on the static pressure at the bottom of a granular column. We make a quantitative analysis of the pressure saturation when the column height is increased. We evidence a great sensitivity of the measurements with the global packing fraction and the eventual presence of shear bands at the boundaries. We also show the limit of the classical Janssen model and discuss these experimental results under the scope of recently proposed theoretical frameworks.

The effect of ethanol vapor adsorption on the properties of porous silicon-based structures was studied by Raman scattering, infrared spectroscopy, and I–V characteristics. A decrease in the resistance of porous silicon layers and a simultaneous increase in the intensity of the band of infrared absorption caused by the presence of (OH) − … x (OH) − ( x = 1, 2, …) groups upon exposure to ethanol vapor and vice versa in the case of degassing were detected. The observed effect is attributed to a change in the depletion region in por-Si skeleton elements due to the electrostatic interaction of (OH) − groups with positively charged surface defects. The effect of hydrogen-bonded Si-OH…OH-C 2 H 5 centers on the increase in the silicon conductivity is discussed.

In structures with a porous buffer layer, residual internal stresses caused by a mismatch between the crystal-lattice parameters of the epitaxial GaInP alloy and the GaAs substrate are redistributed to the porous layer that acts as a buffer and is conducive to disappearance of internal stresses. Doping of the epitaxial layer with dysprosium exerts a similar effect on the internal stresses in the film-substrate structure.

The effect of rapid thermal annealing on the structural and physical properties of Au-(Ti, Zr)B x -GaN(SiC) contacts and diode structures on their basis is investigated. The X-ray-diffraction investigations and the layer-by-layer Auger analysis showed that the phase composition and structure of the GaN and SiC contacts are retained to the temperatures as high as 900 and 1000°C, respectively. The stability of interphase boundaries is confirmed by almost constant physical properties of contacts before and after the rapid thermal treatments. The Schottky-barrier height φ b amounts to 0.89–0.9 eV for the contacts with GaN and 0.79–0.83 eV for SiC; the ideality factor n of the I–V characteristic amounts to n = 1.2 for the Au-TiB x (ZrB x )- n -GaN(SiC) contacts and n ≈ 1.12 for the Au-ZrB x - n - n + -4 H SiC contacts. The structural investigations indicate that there are glass-forming boron and metal oxides at an interphase boundary, which form a thin amorphous vitreous layer resistant against rapid thermal annealing and represent the diffusion barrier for the interphase transport.

We show that two basic mechanical processes, the collision of particles and rolling motion of a sphere on a plane, are intimately related. According to our recent findings, the restitution coefficient for colliding spherical particles , which characterizes the energy loss upon collision, is directly related to the rolling friction coefficient for a viscous sphere on a hard plane. We quantify both coefficients in terms of material constants which allows to determine either of them provided the other is known. This relation between the coefficients may give rise to a novel experimental technique to determine alternatively the coefficient of restitution or the coefficient of rolling friction.