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"Adhesive bonding"
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A Review of Structural Adhesive Joints in Hybrid Joining Processes
by
Maggiore, Sofia
,
Stagnaro, Paola
,
Banea, Mariana D.
in
Adhesive bonding
,
Adhesive joints
,
Bond strength
2021
Hybrid joining (HJ) is the combination of two or more joining techniques to produce joints with enhanced properties in comparison to those obtained from their parent techniques. Their adoption is widespread (metal to metal joint, composite to composite and composite to metal) and is present in a vast range of applications including all industrial sectors, from automotive to aerospace, including naval, construction, mechanical and utilities. The objective of this literature review is to summarize the existing research on hybrid joining processes incorporating structural adhesives highlighting their field of application and to present the recent development in this field. To achieve this goal, the first part presents an introduction on the main class of adhesives, subdivided by their chemical nature (epoxy, polyurethane, acrylic and cyanoacrylate, anaerobic and high-temperature adhesives) The second part describes the most commonly used Hybrid Joining (HJ) techniques (mechanical fastening and adhesive bonding, welding processes and adhesive bonding) The third part of the review is about the application of adhesives in dependence of performance, advantage and disadvantage in the hybrid joining processes. Finally, conclusions and an outlook on critical challenges, future perspectives and research activities are summarized. It was concluded that the use of hybrid joining technology could be considered as a potential solution in various industries, in order to reduce the mass as well as the manufacturing cost.
Journal Article
Low Temperature Adhesive Bonding-Based Fabrication of an Air-Borne Flexible Piezoelectric Micromachined Ultrasonic Transducer
2020
This paper presents the development of a flexible piezoelectric micromachined ultrasonic transducer (PMUT) that can conform to flat, concave, and convex surfaces and work in air. The PMUT consists of an Ag-coated polyvinylidene fluoride (PVDF) film mounted onto a laser-manipulated polymer substrate. A low temperature (<100 °C) adhesive bonding technique is adopted in the fabrication process. Finite element analysis (FEA) is implemented to confirm the capability of predicting the resonant frequency of composite diaphragms and optimizing the device. The manufactured PMUT exhibits a center frequency of 198 kHz with a wide operational bandwidth. Its acoustic performance is demonstrated by transmitting and receiving ultrasound in air on curved surface. The conclusions from this study indicate the proposed PMUT has great potential in ultrasonic and wearable devices applications.
Journal Article
Creep Crack Growth Behavior during Hot Water Immersion of an Epoxy Adhesive Using a Spring-Loaded Double Cantilever Beam Test Method
by
Kazumasa Shimamoto
,
Chiaki Sato
,
Kota Nakamura
in
Adhesive bonding
,
adhesive bonding; hydrothermal creep; degradation; creep fracture toughness; aging
,
Adhesive joints
2023
Double cantilever beam (DCB) tests were conducted by immersing the specimens in temperature-controlled water while applying a creep load using a spring. By introducing a data reduction scheme to the spring-loaded DCB test method, it was confirmed that only a single parameter measurement was sufficient to calculate the energy release rate (ERR). Aluminum alloy substrates bonded with an epoxy adhesive were used, and DCB tests were performed by changing the initial load values, spring constants, and immersion temperatures for two types of surface treatment. The initial applied load and spring constant had no effect on the ERR threshold. In contrast, the threshold decreased with the increasing immersion temperature, but even in the worst case, it was 15% of the critical ERR in the static tests. Using the creep crack growth relationship, it was revealed that there were three phases of creep immersion crack growth in the adhesive joints, and each phase was affected by the temperature. The spring-loaded DCB test method has great potential for investigating the combined effects of creep, moisture, and temperature, and this study has demonstrated the validity of the test method. The long-term durability of adhesive joints becomes increasingly important, and this test method is expected to become widespread.
Journal Article
Influence of Pre-Treatment and Artificial Aging on the Retention of 3D-Printed Permanent Composite Crowns
2022
The aim of this in vitro study is to investigate the bonding properties of a 3D-printable permanent composite material in comparison to milled composite materials. The tested materials are 3D-printed BEGO VarseoSmile Crown plus (VA1_ab, VA1_nt, VA2_ab, VA2_nt), Vita Enamic (EN1, EN2), and 3M Lava Ultimate (UL1, UL2) (N = 64; n = 8). For this purpose, all crowns are luted to polymer tooth stumps #46 (FDI) using dual-curing luting composite, strictly according to the manufacturer’s instructions. VA1_ab and VA2_ab are additionally airborne-particle abraded. 4 groups (VA2_ab, VA2_nt, EN2, UL2) are artificially aged (1,200,000 cycles, 50 N, 10,000 thermocycles), whereby no specimen has failed. All 64 specimens undergo pull-off testing until retention loss. The mean forces of retention-loss is 786.6 ± 137.6 N (VA1_nt, *), 988.6 ± 212.1 N (VA2_nt, *, Ɨ), 1223.8 ± 119.2 N (VA1_ab, Ɨ, ǂ), 1051.9 ± 107.2 N (VA2_ab, *, Ɨ), 1185.9 ± 211.8 N (EN1, Ɨ, ǂ), 1485.0 ± 198.2 N EN2, ǂ), 1533.8 ± 42.4 N (UL1, ǂ), and 1521.8 ± 343.4 N (UL2, ǂ) (one-way ANOVA (Scheffé method); p < 0.05; *, Ɨ, ǂ: group distribution). No characteristic failure modes can be detected. In conclusion, all of the pull-off forces reflect retention values that seem to be sufficiently high for clinical use. Additional airborne-particle abrasion of VA does not result in significantly better retention but can be recommended.
Journal Article
Comparative Study of Resin and Silane Coupling Agents Coating Treatments on Bonding Strength Improvement of Titanium and Carbon Fiber Composites
2023
In this study, anodizing treatment was utilized to etch titanium (Ti) substrates’ surface to prefabricate nano-cavities. Resin pre-coating (RPC) and three silane coupling agents’ coating (CAC) techniques were further applied to porous Ti substrates surface to compare the reinforcement effect of adhesive bonding strength. SEM images show that nano-cavities have been prepared to create a greater contact area and vertical volume on Ti substrate surface, fully covered by resin coatings via RPC. A higher surface roughness and better surface wetting are also obtained by the testing results of atomic force microscope and contact angles. Single lap shear tests results indicate that specimens with “anodizing + RPC” treatment yield the best average shear strength of 20.73 MPa, increased by 31.7% compared to anodizing base strength and at least 63.0% higher than silane KH-550/560/792-coated specimens. A dominant cohesive failure and fiber-tearing on CFRP’s shallow surface, instead of adhesive debonding failure, are shown in the appearances of damaged specimens, proving that the RPC technique has a more effective bonding strength reinforcement in titanium and carbon fiber-reinforced polymer (Ti-CFRP) composites’ toughening. Thus, the simple RPC technique can be regarded as a new-type alternative to adhesive joint toughening to manufacture high-performance composites for aerospace applications.
Journal Article
Axial Tensile Adhesively Bonded Performance of Carbon Fiber Composite Tubes Under Room-Temperature and Low-Temperature Circulation
2025
This study investigated the axial tensile performance of adhesively bonded T700/C204 carbon fiber composite and TC4 titanium alloy tubular single-lap joints under three distinct temperature conditions: room temperature, low temperature (−65 °C), and room–low–room-temperature cycling. Two configurations of adhesively bonded joints—composite–composite and composite–titanium—were tested. Specimens were designed to evaluate the influence of spew-fillet and perfect lap configurations on uniaxial tensile bonding strength across varying temperature environments. Analysis of the final failure morphology, stress concentration locations, ultimate failure loads, and load-displacement curves revealed that stress concentration and peeling stress were most pronounced at the ends of the bonded region, which served as the initiation points for failure. The adhesively bonded joints exhibited two distinct failure modes, strongly correlated with material properties and environmental temperature. The titanium alloy tubular joints predominantly experienced adhesive layer failure, while the carbon fiber three-way tubular joints were primarily characterized by fiber-tear failure. Environmental temperature significantly influenced the strength of the adhesively bonded joints. Specifically, the tensile failure limit of the bonded specimens subjected to low-temperature cycling (25~−65~25 °C) was approximately 61% higher than that observed under the room or low-temperature conditions. Furthermore, the experimental results demonstrated that a maximum failure load of 27.522 kN and a shear strength of 10.956 MPa were achieved. Notably, the presence of adhesive spew-fillet had a negligible impact on the bonding strength of the joints.
Journal Article
Enhancement of adhesion strength by micro-rolling-based surface texturing
2015
Structural adhesive bonding technology is widely utilized in various applications in modern automotive and aviation industries. Finding new techniques to enhance adhesion strength between bonded components in a more economical and environmental-friendly way is becoming an important issue. In this paper, a novel micro-surface texturing method by using a developed deformation-based micro-rolling system has been applied to modify surface conditions of a sheet metal in order to increase metal-to-metal adhesion strength. Additionally, different surface texturing patterns, such as micro-channel arrays and grid pattern, are produced by single-pass or two-pass micro-rolling strategies. The effect of these texture patterns on adhesion strength is studied through single-lap-joint shear strength test. Results indicate that surface with micro-textures are able to achieve noticeable improvement in adhesion strength.
Journal Article
Degradation of structural adhesive bonding joints on ship exposure decks
2020
The degradation process of adhesive bonding layers on ship exposure decks was examined via an exposure test using adhesive bonding joint specimens under tensile shear load. The degradation was evaluated by the delamination and the deformation of the adhesive layer. The degradation initiated in summer, which was more significant for the specimens located at exposed areas of the ship than those in the engine room (i.e. not exposed area). Environmental measurements revealed that, in summer, the daily highest surface temperature was greatly raised at the exposed areas that, however, exhibited equal or lower average values compared to the engine room. The degradation of an adhesive bonding joint would initiate relatively rapidly in a high-temperature environment. This indicates the highest temperature is a more important factor for adhesive bonding durability than the average temperature. The tensile test conducted after the exposure test showed that the degradation progressed from the adhesive layer edge. The surface temperature on an ocean-going ship was also measured to examine the temperature condition, revealing more severe values than those on ships in mid-latitude regions such as Japan. The design temperature for adhesive bonding joints should be estimated as at least 70 °C for exposed areas.
Journal Article
Influence of Dry-Film Lubricants on Bond Strength and Corrosion Behaviour of 6xxx Aluminium Alloy Adhesive Joints for the Automotive Industry
by
Stifter, David
,
Gruber, Ralph
,
Bruckner, Thomas Maximilian
in
accelerated corrosion testing
,
Adhesive bonding
,
Adhesive joints
2023
In the automotive industry, the application of dry lubricants on aluminium is indispensable for achieving a high-quality forming behaviour. To provide a short production time, these forming aids are not removed during the joining step. The aim of this study is the characterisation of the influence of dry lubricants on the bond strength and the corrosion resistance of a 6xxx aluminium alloy for automotive applications. For this purpose, samples with a well-defined surface were coated with 1 g/m2 dry lubricant and joined with a commercial thermosetting 1K epoxy structural adhesive. The bond strength was measured with lap shear tests. To evaluate the corrosion resistance of the adhered aluminium samples, an immersion test in a 5 wt.% NaCl solution was used. Based on the fracture pattern analysis, the corrosion behaviour could be described, and the possible corrosion mechanisms are proposed. The influence of the load quantity of the dry lubricants is observed microscopically and mechanically. The environmentally induced degradation process of the adhesive is examined by an investigation of the volumetric change during the testing and with scanning electron microscopy. Using a simulation, the changes in the adhesive polymer matrix at the metal–adhesive interface caused by the dry lubricants are examined using polymer test procedures like dynamic mechanical analysis, differential scanning calorimetry and tensile tests. The results show a significant effect of the forming aid on the corrosion resistance of the adhered aluminium samples against the corrosive infiltration of the metal–adhesive interface.
Journal Article
Aerosol Jet Printing and Interconnection Technologies on Additive Manufactured Substrates
by
Jaeger, Jonas
,
Eberhardt, Wolfgang
,
Werum, Kai
in
Additive manufacturing
,
Adhesive bonding
,
aerosol jet
2022
Nowadays, digital printing technologies such as inkjet and aerosol jet printing are gaining more importance since they have proven to be suitable for the assembly of complex microsystems. This also applies to medical technology applications like hearing aids where patient-specific solutions are required. However, assembly is more challenging than with conventional printed circuit boards in terms of material compatibility between substrate, interconnect material and printed ink. This paper describes how aerosol jet printing of nano metal inks and subsequent assembly processes are utilized to connect electrical components on 3D substrates fabricated by Digital Light Processing (DLP). Conventional assembly technologies such as soldering and conductive adhesive bonding were investigated and characterized. For this purpose, curing methods and substrate pretreatments for different inks were optimized. Furthermore, the usage of electroless plating on printed metal tracks for improved solderability was investigated. Finally, a 3D ear mold substrate was used to build up a technology demonstrator by means of conductive adhesives.
Journal Article