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The paper presents results of experimental investigations of the influence of temperature on the effectiveness of passive vibration isolation. Two types of viscoelastic materials (butyl rubber and bituminous material) were tested. In the performed vibration analysis, the Oberst beam made out of aluminum alloy with a damping material in a Free Layer Damping (FLD) configuration was used. The experimental modal analysis was performed using the Unholtz-Dickie UDCO TA-250 vibration system. To investigate the influence of temperature on the effectiveness of passive vibration isolation, an isothermal cooling chamber (using Peltier cells) was designed and constructed. The tests were carried out in a wide frequency range from 40 Hz to 4000 Hz, at a constant sweep rate, in a temperature range from −2 °C to 22 °C. Miniature piezoelectric acceleration sensors were used to determine the acceleration of the beam and the exciter head. The analysis of accelerations of both the object and the shaker head allowed for the determination of a Frequency Response Function (FRF) for the beam. The course of FRF was used to determine the resonance frequencies and the vibration amplitudes of the beam damped with bituminous material and butyl rubber at various temperatures. The loss factor η, calculated for each resonance using the generalized half-power method (n-dB method), was used as an indicator of damping intensity. The research results presented in this work (important from scientific point of view) also have utilitarian significance and can be used in the design of more quiet and comfortable motor vehicles, railway wagons and aircraft structures.

The objective of this work is to improve the viscoelastic properties of local AC-20 asphalt. Ecuador has a nano clay deposit arranged in 6 levels from A1-A6, in an area of 4000 [km.sup.2]. Those nano clays were treated with chemical and physical methods, using a) NaOH, b) N[H.sub.3], [H.sub.2][O.sub.2] (molar ratio 5), and c) calcination to obtain an effective additive to be mixed with the bitumen. 532 samples were prepared, and their viscoelastic properties were measured with the dynamic shear rheometer (DSR) in the first stage. In the second stage, the best hot mix asphalt (HMA) samples were selected, and the parameters of mixing time, mixing speed, calcination temperature, and additive concentration were optimized. It was discovered that nano clay A1 calcined in the 270-275[degrees]C window activated its high level of adsorption, becoming the best additive (S1) for HMA hot asphalt mixtures. The use of 3% S1 + AC-20 and mixing times (MT) of 30, 60, 90 and 120 minutes allowed the complex modulus (G*) to increase up to 305.5%, while the phase angle S decreased by -8.37% (MT= 90 min). The performance grade improved from PG= 64 (original) to 70, 76, and 82. These results agree with the significant adsorption capacity that this material presents.

This study explores the integration of copper oxide (Cu[sub.2]O) into bitumen and leverages Artificial Intelligence (AI) to evaluate and optimize the binder’s performance across multiple scales. Comprehensive laboratory tests, including conventional binder properties, rheological analysis, aging simulations, low-temperature cracking, and moisture susceptibility, were conducted on base and Cu[sub.2]O modified asphalt binders. The results were used to train predictive models using gradient boosting regressors for each performance category. Optimization identified ideal Cu[sub.2]O ratios for different engineering goals, offering practical recommendations. Based on this integrated cost-performance analysis, a Cu[sub.2]O concentration of 2.3% was recommended as the most efficient trade-off point. AI modeling using Gradient Boosting Regressor (GBR) achieved high predictive performance, with R[sup.2] values reaching 0.98 for BBR prediction and 0.78 for rheology, and mean absolute error (MAE) values as low as 4.21. This demonstrates the model’s robustness in capturing complex nonlinear binder behaviors.

This research utilized recycled acetate fibers from discarded cigarette butts (CBs) as reinforcing materials, reducing solid waste and enhancing the properties of bitumen. The surface properties of the fibers significantly impacted the binder characteristics. The treatment of CB fibers with anhydrous ethanol was employed to remove the plasticizer glycerol triacetate (GTA), enabling the better homogeneity of the fibers in the binder. Thermogravimetric analysis (TGA) and scanning electron microscopy (SEM) were used to assess the effectiveness of the fiber treatment. A dynamic shear rheometer (DSR) was used to explore the properties of bitumen with varying CB contents (0%, 0.25%, 0.75%, and 1.25% by weight). A whole life cycle analysis further confirmed the eco-efficiency of CB binders. The results show that the pretreatment effectively removed GTA, leading to a more homogeneous dispersion of fibers in the binder. Adding CBs can significantly improve bitumen properties, but this effect does not increase with higher dosages; when the CB content exceeded 1.25%, a reduction in fatigue resistance was observed. Among the tested dosages, the optimal amount was 0.75%, which improved the high-temperature performance of the binder by 2.7 times, the medium-temperature fatigue life by 1.78 times, and the low-temperature performance by 1.08 times. In terms of ecological benefits, the addition of CB fibers to bitumen pavement reduced carbon emissions by two-thirds compared to traditional bitumen pavement, resulting in a significant decrease in carbon emissions. This study provides valuable insights into the construction of sustainable transportation infrastructure.

The carbon footprint reduction mandate and other eco-friendly policies currently in place are constantly driving the trend of the synthesis and application of sustainable functional materials. The bitumen industry is not an exception to this trend and, every day, new technologies that facilitate safer, cost effective and more sustainable industrial processes and road paving operations are being researched and brought to light. A lot of research is currently ongoing to improve bitumen’s properties due to its use as a binder in road paving processes. Over the years, the most common method to improve bitumen’s properties has been with the use of additives. The major drawback in the use of these additives is the fact that they are substances of strong chemical nature which are either too acidic, too basic or emit toxic fumes and volatile organic compounds into the environment. In the long run, these chemicals are also toxic to the road pavement personnel that carry out the day to day industrial and paving operations. This led researchers to the initiative of synthesizing and applying biomaterials to be used as additives for bitumen. In this light, several studies have investigated the use of substances such as bio-oils, natural waxes, gum, polysaccharides and natural rubber. This literature review is aimed at classifying the different bio-based materials used to improve bitumen’s properties and to provide a deeper knowledge of the application of these biomaterials in bitumen technology. In general, we highlight how the research efforts elaborated herein could potentially foster safer, sustainable, eco-friendly approaches to improving bitumen’s properties while also promoting a circular economy.

The circular economy (i.e., reuse and recycling of waste materials) is gaining attention for the goal of achieving net-zero waste. In this regard, the use of waterproofing membrane waste in bituminous materials can be a valid option, as every year, a lot of bituminous membrane wastes are generated both as production scraps or end-of-life wastes. Given this background, the recycling feasibility of end-of-life bituminous membrane waste (MW) in asphalt mixtures was assessed in this research study. To this aim, MW shreds (≤20 mm) were added to dense-graded bituminous mixtures using the dry-mixing method. The shreds were dosed at 0.5% by the mix weight (mix coded as SH−) or at 2% by mix weight (mix coded as SH+). A corresponding reference mix without MW was also tested for comparison purposes. The mixtures’ workability, strength and stiffness as well as permanent deformation, moisture and fatigue resistance were evaluated. Overall, the laboratory experimental findings showed that MW-modified bituminous mixtures with a higher dosage of membrane waste (SH+) have relatively higher moisture resistance, fatigue resistance, stiffness and high-temperature performance with respect to the corresponding reference mix. Moreover, both the reference and MW-modified mixtures showed similar workability regardless of the MW content.

Straipsnyje aprasomas polimeru modifkuoto keliu bitumo regeneravimo dvieju rusiu atnaujinanciosiomis medziagomis efektyvumas. Pasirinktos dvi alternatyvios atnaujinanciosios medziagos - aromatine alyva Nygen 910 ir minkstasis keliu bitumas V12000. Tirtas PMB 45/80-55 bitumas, kuris naudojamas asfalto dangos virsutiniuose ir apatiniuose sluoksniuose. Asfalto dangos eksploatacijos metu del saules UV radiacijos, temperaturos ir aplinkos deguonies poveikio asfalto virsutinis sluoksnis pasiekia didziausia senejimo laipsni is visu konstrukcijos sluoksniu. Bitumo senejimui laboratorijos salygomis imituoti atliktas trumpalaikis ir pagreitintas ilgalaikis sendinimas. Siekiant nustatyti optimalu atnaujinanciosios medziagos kieki eksperimentai atlikti su 8 %, 10 % ir 14 % atnaujinanciosios medziagos nuo bitumo mases. Atnaujinanciuju medziagu poveikis vertintas tiriant pagrindines bitumo fzikines savybes: penetracija ir minkstejimo temperatura. Eksperimentinio tyrimo metu nustatyta, kad aromatine alyva yra daugiau nei 2,5 karto efektyvesne nei minkstas bitumas.

Natural bitumens consist of many molecules whose chemical composition depends on the oilfield and determines the physicochemical properties of the bitumens as materials. Infrared (IR) spectroscopy is the fastest and least expensive method to assess the chemical structure of organic molecules, which makes it attractive in terms of rapid prediction of the properties of natural bitumens based on their composition evaluated in this way. In this work, IR spectra were measured for ten samples of natural bitumens significantly different in properties and origin. Based on the ratios of certain IR absorption bands, bitumens are proposed to be divided into paraffinic, aromatic, and resinous. In addition, the internal relationship between IR spectral characteristics of bitumens, such as polarity, paraffinicity, branchiness, and aromaticity, is shown. A study of phase transitions in bitumens by differential scanning calorimetry was carried out, and the use of a heat flow differential to find hidden points of bitumens’ glass transitions is proposed. Furthermore, the dependences of the total melting enthalpy of crystallizable paraffinic compounds on the aromaticity and branchiness of bitumens are demonstrated. A detailed study of bitumens’ rheology in a wide temperature range was carried out, and characteristic features of rheological behavior for different bitumen classes are revealed. Based on the viscous properties of bitumens, their glass transition points were found and compared with the calorimetric glass transition temperatures and nominal solid–liquid transition points obtained from temperature dependences of bitumens’ storage and loss moduli. The dependences of viscosity, flow activation energy, and glass transition temperature of bitumens on their IR spectral characteristics are shown, which can be used to predict the rheological properties of bitumens.

This study investigated the suitability of recycled asphalt pavement and polyethylene wastes as coarse aggregate in asphaltic concrete by evaluating the impact of the use of polyethylene polymer wastes and recycled asphalt pavement composite as aggregates on the physical and mechanical properties of the asphaltic concrete. The physical characteristics of the aggregate and bitumen were determined using relevant parametric tests. Recycled asphalt pavement was used to make asphaltic concrete samples using LDPE at 5%, 10%, 15%, RAP at 5% and HDPE at 5%, 10%, 15%, and a mixture of LDPE + HDPE at 5+5%, 7.5+7.5% and 10+10% RAP at 5% as additives. Marshall Stability test was conducted to assess the mechanical strength of the asphaltic concrete, and the results included information on the aggregate’s stability, flow, density, voids filled with bitumen, voids filled with air, and voids in mineral aggregate. In addition, the surface and crystal structure of the aggregates was studied by carrying out a microscopic examination with a Scanning Electron Microscope (SEM) and X-Ray diffraction (XRD). The results obtained from this study demonstrated that RAP, HDPE & LDPE are viable conventional aggregate substitute for asphalt concrete production.

Douglas Channel and the adjacent Hecate Strait (British Columbia, Canada) are part of a proposed route to ship diluted bitumen (dilbit). This study presents how two types of dilbit naturally degrade in this environment by using an in situ microcosm design based on dilbit-coated beads. We show that dilbit-associated n-alkanes were microbially biodegraded with estimated half-lives of 57-69 days. n-Alkanes appeared to be primarily degraded using the aerobic alkB, IadA and CYP153 pathways. The loss of dilbit polycyclic aromatic hydrocarbons (PAHs) was slower than of n-alkanes, with half-lives of 89-439 days. A biodegradation of PAHs could not be conclusively determined, although a significant enrichment of the phnAc gene (a marker for aerobic PAH biodegradation) was observed. PAH degradation appeared to be slower in Hecate Strait than in Douglas Channel. Microcosm-associated microbial communities were shaped by the presence of dilbit, deployment location and incubation time but not by dilbit type. Metagenome-assembled genomes of putative dilbit-degraders were obtained and could be divided into populations of early, late and continuous degraders. The majority of the identified MAGs could be assigned to the orders Flavobacteriales, Methylococcales, Pseudomonadales and Rhodobacterales. A high proportion of the MAGs represent currently unknown lineages or lineages with currently no cultured representative.