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Owing to superior physio-chemical characteristics, titanium alloys are widely adopted in numerous fields such as medical, aerospace, and military applications. However, titanium alloys have poor machinability due to its low thermal conductivity which results in high temperature during machining. Numerous lubrication and cooling techniques have already been employed to reduce the harmful environmental footprints and temperature elevation and to improve the machining of titanium alloys. In this current work, an attempt has been made to evaluate the effectiveness of two cooling and lubrication techniques namely cryogenic cooling and hybrid nanoadditive–based minimum quantity lubrication (MQL). The key objective of this experimental research is to compare the influence of cryogenic CO 2 and hybrid nanofluid–based MQL techniques for turning Ti–6Al–4V. The used hybrid nanofluid is alumina (Al 2 O 3 ) with multi-walled carbon nanotubes (MWCNTs) dispersed in vegetable oil. Taguchi-based L9 orthogonal-array was used for the design of the experiment. The design variables were cutting speed, feed rate, and cooling technique. Results showed that the hybrid nanoadditives reduced the average surface roughness by 8.72%, cutting force by 11.8%, and increased the tool life by 23% in comparison with the cryogenic cooling. Nevertheless, the cryogenic technique showed a reduction of 11.2% in cutting temperature compared to the MQL-hybrid nanofluids at low and high levels of cutting speed and feed rate. In this regard, a milestone has been achieved by implementing two different sustainable cooling/lubrication techniques.

Owing to poor thermal conductivity, heat dissipation, and high chemical reactivity toward most of the tool materials, temperature elevation in the machining of titanium alloy leads to poor surface quality. Based on analyzing the variation laws of the milling forces under cryogenic cooling, the present investigation concerns the surface integrity (surface roughness, micro-hardness, microstructures, and residual stresses) in cryogenic milling of Ti-6Al-4 V alloy under the application of liquid nitrogen (LN 2 ) as a cooling mode. Findings have indicated a dramatic increase in milling forces, and decreasing surface roughness was observed under variation of jet temperature (20~−196 °C). Besides an increase in cutting speed from 60 to 120 m/min, a linear increase in cutting forces, surface roughness, micro-hardness, and residual compressive stress was observed. The minimum micro-hardness decreased at cutting speed of 90 m/min and up to 30 μm in depth. A holistic comparison between obtained results under cryogenic milling and previously studied results under dry milling at same cutting conditions depicted higher micro-hardness and higher compressive residual stress under cryogenic LN 2 on the machined surface. However, the residual stress under LN 2 cooling conditions tends to decrease relatively slower compared to dry milling. Also, there are no significant differences in grain refinement and twisting under dry and cryogenic LN 2 machining. The research work proves the effectiveness of cryogenic milling in improving the surface integrity of the Ti-6Al-4 V alloy.

Although high-entropy alloys (HEAs) are attracting interest, the physical metallurgical mechanisms related to their properties have mostly not been clarified, and this limits wider industrial applications, in addition to the high alloy costs. We clarify the physical metallurgical reasons for the materials phenomena (sluggish diffusion and micro-twining at cryogenic temperatures) and investigate the effect of individual elements on solid solution hardening for the equiatomic CoCrFeMnNi HEA based on atomistic simulations (Monte Carlo, molecular dynamics and molecular statics). A significant number of stable vacant lattice sites with high migration energy barriers exists and is thought to cause the sluggish diffusion. We predict that the hexagonal close-packed (hcp) structure is more stable than the face-centered cubic (fcc) structure at 0 K, which we propose as the fundamental reason for the micro-twinning at cryogenic temperatures. The alloying effect on the critical resolved shear stress (CRSS) is well predicted by the atomistic simulation, used for a design of non-equiatomic fcc HEAs with improved strength, and is experimentally verified. This study demonstrates the applicability of the proposed atomistic approach combined with a thermodynamic calculation technique to a computational design of advanced HEAs.

There has been a substantial growth in using carbon fiber-reinforced plastic (CFRP) composite materials in aerospace and automotive industries due to their superior properties. This experimental study presents results from a comprehensive and systematic study investigating the effects of cryogenic cooling on drilling performance and surface integrity characteristics of CFRP composite material. Experimental data on cutting edge radius of drill bit, outer corner wear of drill bit, trust force, torque, delamination factor, and surface integrity characteristics, including borehole subsurface damage and diameter error of drilled hole, are presented and analyzed comparing dry drilling with cryogenic cooling of CFRP composite material. The findings demonstrate that cryogenic cooling has a profound effect on reducing the cutting edge rounding of drill bit and outer corner wear; it also helps enhancing the surface integrity characteristics of produced hole. However, cryogenic cooling generates larger thrust force, torque, and thus larger delamination factor.

In this study, the effect of both cryogenic and dry machining of AZ31 magnesium alloy on temperature and surface roughness was examined. Cryogenic machining experiments were conducted by applying liquid nitrogen at the cutting zone. The cutting parameters (cutting speed, depth of cut, and feed rate) were varied, and their effect on the results was identified. It was found that the cryogenic machining was able to reduce the maximum temperature at the machined surface to about 60% as compared with dry machining. A finite element model was developed to predict the temperature distribution at the machined surface. The simulated results showed good agreement with the experimental data. After analyzing the temperature distribution, the model also suggested that the cryogenic-assisted machining removes heat at a faster rate as to that of the dry machining. An arithmetic model using the response surface method was also developed to predict the maximum temperature at the surface during cryogenic and dry machining. The analysis pointed out that the maximum temperature was greatly affected by the cutting speed followed by feed rate and depth of cut. Cryogenic machining leads to better surface finish with up to 56% reduction in surface roughness compared with dry machining.

The 2195 aluminum alloy is widely used in cryogenic storage tanks for space vehicles, where it can reach a temperature of 20 K. In order to explore the reasons for the increased strength of 2195 aluminum alloys at cryogenic temperatures, uniaxial tensile tests were conducted in the range of 20 K–298 K. Tensile fracture was observed. In addition, the microstructures under different temperatures were observed using EBSD (electron back-scattered diffraction) and TEM (transmission electron microscopy) techniques, and the dislocation density of the material was quantitatively characterized using the modified Williamsone–Hall method based on XRD (X-ray diffraction) analysis. The results indicated that the ultimate strength increased at an increasing rate with the temperature decrease, while the elongation increase was insignificant. The fracture’s surface exhibited that dimple characteristics seemed to be unapparent while the quantity of tearing ridges was enhanced by the temperature decrease. Meanwhile, the fracture mode changed from ductile to brittle fracture. The microdeformation degree revealed by KAM images showed an aggravating trend, and the deformation tended to be more uniform. The increasingly enhanced dislocation density quantitatively revealed by the modified Williamsone–Hall method also proved this and that the increase in dislocations had a similar trend to that of tensile strength, which was furtherly revealed by TEM images. This indicated that the more regions are involved in deformation, the more dislocations are generated in the material during deformation, resulting in an increase in strength at cryogenic temperatures.

We present sample transfer instrumentation and integrated protocols for the preparation and atom probe characterization of environmentally-sensitive materials. Ultra-high vacuum cryogenic suitcases allow specimen transfer between preparation, processing and several imaging platforms without exposure to atmospheric contamination. For expedient transfers, we installed a fast-docking station equipped with a cryogenic pump upon three systems; two atom probes, a scanning electron microscope / Xe-plasma focused ion beam and a N2-atmosphere glovebox. We also installed a plasma FIB with a solid-state cooling stage to reduce beam damage and contamination, through reducing chemical activity and with the cryogenic components as passive cryogenic traps. We demonstrate the efficacy of the new laboratory protocols by the successful preparation and transfer of two highly contamination- and temperature-sensitive samples-water and ice. Analysing pure magnesium atom probe data, we show that surface oxidation can be effectively suppressed using an entirely cryogenic protocol (during specimen preparation and during transfer). Starting with the cryogenically-cooled plasma FIB, we also prepared and transferred frozen ice samples while avoiding significant melting or sublimation, suggesting that we may be able to measure the nanostructure of other normally-liquid or soft materials. Isolated cryogenic protocols within the N2 glove box demonstrate the absence of ice condensation suggesting that environmental control can commence from fabrication until atom probe analysis.

The integration of machining as a post-processing method for additive manufacturing (AM) can promote the industrialization of AM and enable it to meet the requirements of high-value industries. This integration introduces several challenges for the machining process, which are related to process design and planning. A major aspect that requires investigation is the cooling of the machining process. Effective cooling is a key part of the machining process, especially when hard materials with low machinability are involved, which is the case with parts built by AM. However, oil-based coolants cannot be utilized in the context of hybrid manufacturing because they contaminate the surface of the part that can lead to the introduction of defects in a successive AM process. Cryogenic cooling is a high-performance and sustainable cooling approach that can be employed to overcome this issue, since it provides a clean surface after the machining process. Although cryogenic cooling is a very promising and sustainable alternative for high-performance cooling, most studies only investigate limited benefits that it can provide in the machining process. Therefore, this paper aims to provide a full overview of the effect of cryogenic cooling with liquid nitrogen (LN 2 ) during milling of Directed Energy Deposited IN718 samples, examining the cutting forces, tool wear, surface roughness and residual stresses on the machined components. The results prove that cryogenic cooling can reduce significantly the cutting forces and tool wear, while its impact on the surface roughness is limited.

Residual stress induced by solution treatment in 6061 aluminum alloy can lead to workpiece deformation, or even premature failure. The efficiency of traditional heat treatment for relieving residual stress is relatively low. Therefore, this study introduces a novel cryogenic treatment technique to reduce residual stress. The optimal cryogenic process parameters were achieved by orthogonal experiments: cryogenic temperature of 113 K, holding time of 24 h, 1 cryogenic cycle, and a cooling rate of 3 K·min−1, and the residual stress of aluminum alloy was measured by the blind hole method. The microstructural evolutions in 6061 aluminum alloy were tested by OM, SEM, and TEM. The results show that the introduction of cryogenic treatment can reduce residual stress in 6061 aluminum alloy by 64%, mainly due to the reduction of dislocations and the uniform distribution of β’’ phase.

In this study, Taguchi method has been applied to evaluate the effect of cryogenically treated tools in turning of Hastelloy C22 super alloy on surface roughness. The optimum parameters (cryogenic treatment, cutting speed, and feed rate) of turning were determined by using the Taguchi experimental design method. In Taguchi method, L9 orthogonal array has been used to determine the signal noise (S/N) ratio. Analysis of ANOVA was carried out to identify the significant factors affecting surface roughness. The statistical analysis indicated that feed rate, with a contribution percentage as high as 87.64 %, had the most dominant effect on machining performance, followed by the cryo-treated tools treatment and cutting speed, respectively. The confirmation tests indicated that it is possible to improve surface roughness significantly by using the Taguchi method. Surface roughness was improved by 28.3 and 72.3 % by shallow (CT1) cryogenic treatment and deep cryogenic treatment (CT2) applied on cementite carbide tools (UT). It found that wear resistance of tungsten carbide insert was increased by shallow and deep cryogenic treatments.