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\"This may be the best discovery to come out of Nevada mining since the Big Bonanza vein itself. Dan De Quille was the outstanding reporter of the Comstock Lode, and almost anything he would have to say about it would be worth reading.\"--Michael Green.

As high-grade gold deposits are progressively depleted, the proportion of refractory gold ores in total reserves is continuously increasing, making gold recovery from refractory ores an inevitable trend in the future development of the gold industry. This study briefly analyzes the challenges faced during the leaching process of refractory gold ores under ambient conditions, and provides a detailed discussion on two acidic pretreatment technologies—pressure oxidation and bio-oxidation—as well as three acidic gold recovery technologies—thiosulfate leaching process, halogen leaching process, and thiocyanate leaching process. Additionally, this paper compares and analyzes the advantages and limitations of these acidic pretreatment and hydrometallurgical gold recovery technologies. The goal is to provide a comprehensive review of pretreatment technologies and leaching agents for refractory gold ores under acidic conditions (pH = 1–5), offering a reference for selecting appropriate treatment processes in the future, and to explore the potential development of acidic pretreatment and recovery technologies for refractory gold ores.

Timing of the major Baiyun gold deposit (~ 70 t Au) in the northeastern North China Craton is controversial. A textural and geochronological study of high-grade gold ores identifies three generations of xenotime (Xtm-1, Xtm-2 and Xtm-3), even in single grains. The oldest Xtm-1, in grain cores, is of metamorphic origin, with very high U and U/Th ratios, and hump-shaped, HREE-enriched patterns with maximum normalized values at Yb and large negative Eu anomalies. It is dated at 1856 ± 6 Ma, consistent with its crystallization during regional metamorphism related to cratonization. In contrast, 244 ± 2 Ma Xtm-2 overgrowths are of hydrothermal origin, having low U and U/Th ratios and hump-shaped, MREE-enriched patterns with maximum normalized values at Ho and negligible Eu anomalies. Xtm-2 records a previously unrecognized Middle Triassic hydrothermal episode. Xtm-3, in equilibrium with native gold-hosting pyrite and rutile, is also hydrothermal. The Xtm-3 domains have similar U, U/Th ratios, and MREE-enriched patterns to Xtm-2, but a younger crystallization age of 231 ± 1 Ma. Associated rutile grains that show close textural associations with auriferous pyrite and native gold have an in situ SIMS U–Pb an intercept age of 229 ± 4 Ma, consistent with that of Xtm-3. Collectively, these reliable ages indicate that gold mineralization at Baiyun occurred at ca. 230 Ma, predating the emplacement of granite intrusions by more than 3 million years. Both the Middle Triassic hydrothermal event (~244 Ma) and the Late Triassic gold mineralization event (~230 Ma) lie within the temporal window of collisional tectonics in the host orogen. In combination, the new geochronology and fluid-inclusion and geological data support Bayun’s classification as an orogenic gold deposit.

This study investigated the flotation performance of W8, a blended xanthate collector containing ethyl, butyl, propyl, and amyl xanthates, combined with ammonium dibutyl dithiophosphate (ADD) for treating low-grade arsenopyrite-type gold ore from Golmud, Qinghai. Real ore flotation tests demonstrated the superior efficacy of the W8 + ADD system, achieving 84.06% gold recovery with 0.34 g/t tailings, outperforming conventional sodium amyl xanthate (SAX) + ADD and sodium propyl xanthate (SPX) + ADD systems. Systematic studies on pure arsenopyrite revealed a significant synergistic effect in the mixed SPX-SAX system (1:4 ratio), representative of W8 composition. At pH 9, the mixed collector achieved 73.5% recovery, substantially higher than individual SPX (37.5%) or SAX (45.8%). This enhanced performance was attributed to improved surface hydrophobicity (contact angle 47.68° vs. 36.92° for SAX), greater adsorption density (4.97 × 10−7 mol/g under depressant conditions), and extensive formation of molecular aggregates observed via AFM, which increased surface roughness to 28.95 nm. Flotation kinetics further confirmed the advantage of W8 + ADD, which reached 72.1% cumulative recovery in 420 s, exceeding both mixed SPX/SAX (69.5%) and single SAX (65.5%) systems. The synergistic interaction among different xanthate components in W8 enables efficient recovery of gold from this refractory ore.

In mining industries, biomining (comprising biooxidation and bioleaching) is implemented to extract metals from specific ores and waste streams with less environmental effect and expense. Usually, micron-sized gold particles are held in a crystal lattice of iron sulfide minerals and expensively extracted using common approaches. Researchers and industries are interested in developing recent technology and biologically sustainable methods in both pretreatment and further extraction steps for extracting this valuable metal from ores. Diverse studies in biooxidation, as a conventional pretreatment, and biocyanidation, as a new proposed biotechnological method in the downstream gold extraction step, have addressed scientific and technological issues in the extraction of this metal. These two methods have become economically practical by merging high-throughput microbiological data, extraction and recovery process knowledge, and theory validation. However, there is still a gap in the implementation of both the pretreatment method and extraction method due to the consistency and their compatibility with operational recovery conditions. This review brings out the recent biooxidation and biocyanidation improvements, innovation, industry and academic research, and obstacles to gold extraction with a brief explanation to address the recent developments.

Environmentally friendly pretreatment of double refractory gold ores (DRGO) to improve gold recovery without emitting pollutant gas is challenging. Sequential biotreatment, including iron-oxidizing microorganisms to decompose sulfides, followed by the enzymatic decomposition of carbonaceous matter, was recently developed. The effect of acid washing by 1 M HCl for 24 h between two bioprocesses was evaluated using a real double refractory gold ore from the Syama mines, Mali, which includes 24 g/t of Au and 5.27 wt% of carbon with a relatively higher graphitic degree. The addition of the acid washing process significantly improved gold recovery by cyanidation to yield to 84.9 ± 0.7% from 64.4 ± 9.2% (n = 2). The positive effects of acid washing can be explained by chemical alteration of carbonaceous matter to facilitate the accessibility for lignin peroxidase (LiP) and manganese peroxidase (MnP) in cell-free spent medium (CFSM), although the agglomeration was enhanced by an acid attack to structural Fe(III) in clay minerals. Sequential treatment of DRGO basically consists of the oxidative dissolution of sulfides and the degradation of carbonaceous matter prior to the extraction of gold; however, the details should be modified depending on the elemental and mineralogical compositions and the graphitic degree of carbonaceous matter.

Specific computational methods, such as machine learning algorithms, can assist mining professionals in quickly and consistently identifying and addressing classification issues related to mineralized horizons, as well as uncovering key variables that impact predictive outcomes, many of which were previously difficult to observe. The integration of numerical and categorical variables, which are part of a dataset for defining ore grades, is part of the daily routine of professionals who obtain the data and manipulate the various phases of analysis in a mining project. Several supervised and unsupervised machine learning methods and applications integrate a wide variety of algorithms that aim at the efficient recognition of patterns and similarities and the ability to make accurate and assertive decisions. The objective of this study is the classification of gold ore or gangue through supervised machine learning methods using numerical variables represented by grade and categorical variables obtained through drillholes descriptions. Four groups of variables were selected with different variable configurations. The application of classification algorithms to different groups of variables aimed to observe the variables of importance and the impact of each one on the classification, in addition to testing the best algorithm in terms of accuracy and precision. The datasets were subjected to training, validation, and testing using the decision tree, random forest, Adaboost, XGBoost, and logistic regression methods. The evaluation was randomly divided into training (60%) and testing (40%) with 10-fold cross-validation. The results revealed that the XGBoost algorithm obtained the best performance, with an accuracy of 0.96 for scenario C1. In the SHAP analysis, the variable As was prominent in the predictions, mainly in scenarios C1 and C3. The arsenic class (Class_As), present mainly in scenario C4, had a significant positive weight in the classification. In the Receiver Operating Characteristic (ROC) and Area Under the Curve (AUC) curves, the results showed that XGBoost/scenario C1 obtained the highest AUC of 0.985, indicating that the algorithm had the best performance in ore/gangue classification of the sample set. The logistic regression algorithm together with AdaBoost had the worst performance, also varying between scenarios.

Gold production in South Africa is projected to continue its decline in future, and prospects for discovery of new high-grade deposits are limited. Many of the mining companies have resorted to mining and processing low-grade and complex gold ores. Such ores are technically challenging to process, which results in low recovery rates, excessive reagent consumption and high operating costs when compared to free-milling gold ores. In the Witwatersrand mines, options of blending low-grade gold ores with high-grade ores exist. Although it is well known that most of the Witwatersrand gold ores are highly amenable to gold cyanidation, not much is known on the leachability of blended ores, especially the effects of mineralogical and metallurgical variability between different gold ores. In this study, we apply a geometallurgical approach to investigate mineralogical and metallurgical factors that influence the leaching of blended ores in a set of bottle shaker and reactor column tests. Three gold-bearing conglomerate units, so-called reefs, i.e., Carbon Leader Reef, Ventersdorp Contact Reef and the Black Reef, all in the Carletonville goldfield, were sampled. The ores were prepared using a terminator jaw crusher followed by vertical spindle pulverizer (20 kg aliquot) and high-pressure grinding rolls (80 kg aliquot). Mineralogical analysis was conducted using a range of complementary tools such as optical microscopy, QEMSCAN and micro–XCT. The results show that Witwatersrand gold ores are amenable to the process of ore blending. Some of the ores, however, contain impervious inert gangue and reactive ore minerals. Leach solution can only access gold locked in impervious gangue minerals through HPGR-induced pores and/or cracks. The optimum ore blending ratio of the bottle shaker experiments (p80 = − 75 μm) comprises 60% Carbon Leader Reef, 20% Ventersdorp Contact Reef and 20% Black Reef and yields 92% recovered Au over a leach period of 40 h. Blended ores with high carbonaceous material (> 1 wt% carbonaceous material, (Black Reef = 36–60%) yield lower recoveries of 60–69% Au). Ore leaching at the mixed-bed reactor column (− 75 μm and − 5.6/+ 4 mm) yields about 70% over a leach period of two weeks. We therefore suggest that the feasibility of ore blending is strongly controlled by the mineralogy of the constituent ores and that a mixed-bed reactor may be a viable alternative method for leaching of the low-grade Witwatersrand gold ores. Material from certain reefs, such as the Black Reef, has synergistic/antagonistic (nonadditive) blending effects. The overall implication of this study is that ore blending ratios, effects of comminution on mineral liberation, an association of gold with other minerals, and gold adsorption behavior will greatly inform future technology choices in the area of geometallurgy.

Typomorphic features of placer gold of the Anabar region were studied as predictive-exploration criteria. The target of the study was to determine the typomorphic features of placer gold related to the intermediate sources (paleo-placers) and the supposed nearby primary ore occurrences. Two varieties of placer gold were identified. The first variety is well-rounded high-fineness lamellar gold with a highly modified internal structure. This native gold is associated with intermediate sources, Neogene–Quaternary watershed pebble beds. The second type includes slightly rounded gold with a wide variation in fineness (494‰–999‰). Its indicator is a block heterophase internal structure. The set of typomorphic features of this variety of placer gold indicates the vicinity of the primary source, what was the prerequisite for constructing prospecting traverses in order to find ore occurrences. As a result of these studies, hydrothermal-metasomatic formations with gold-sulfide mineralization were identified. The main primary substrate for them is fractured near-fault carbonate rocks of the Cambrian and Vendian–Cambrian age. Along with this, hydrothermalites developed on slightly cemented fine-pebble quartz conglomerates of the Middle Permian age were found in the core of exploration wells. Two types of metasomatic rocks are identified: quartz-potassium feldspar and jasperoid. The main ore minerals were galena and pyrite, different ratios by sites were revealed. Gold was identified in the form of small particles in the carbonate and siliceous substrate of hydrothermal-metasomatic formations. The lithological factor was one of the leading favorable factors for the ore formation due to the presence of near-fault highly permeable fractured carbonate and slightly cemented terrigenous rocks. The structural control of the studied ore occurrences is determined by their localization in the Mayat–Logoy and Dogoy–Kuoy faults of the Molodo–Popigay system of discontinuous faults. We assume a two-stage formation of the gold ore occurrences: during the first stage, the ore components in the form of primary hydrothermal-sedimentary ores in the near-gault zones were formed. The second stage was related to the processes of the Mesozoic tectonic-magmatic activation, when the intrusion of basite dikes initiated the mobilization of ore components the gold-sulfide occurrences were formed in the near-fault zone as a result of silicic-potassic metasomatosis of the carbonate and terrigenous rocks.

—The processes occurring during autoclave oxidation leaching of refractory sulfide gold ore concentrates are discussed. As a result of them, hard-to-remove deposits (crust), which decrease the productivity of the equipment, form on all internal surfaces of autoclaves. The phase composition of the deposits is shown to change from section to section in an autoclave, and the main component of the deposits is found to be potassium jarosite KFe 3 (SO 4 ) 2 (OH) 6 . The mechanism of formation of deposits is analyzed and possible methods to prevent them are discussed.