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"Hardenability"
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Toughened composites : micro and macro systems
\"This book covers micro and macro aspects of toughened composites covering polymer matrix, metal matrix, ceramic matrix and nanomatrix. It gives the reader understanding of composites fabrication, construction, and light weight yet high crack - resistance performance, macroscopic testing supported by microscopic bonding and debonding features, models of stress transfer, and commercial features of developing cheaper yet high quality materials. Features: Focuses on micro/macro aspects of toughening methods and principles of composite materials. Includes all types of composites including polymer matrix, metal matrix, ceramic matrix and nanomatrix. Covers corrosion resistance and oxidation resistance as well as solubility resistance. Discusses use of recycled materials. Provides good balance of long fiber, short fiber, nanoparticle, and particulate modifiers. This book aims at Researchers and professionals in Materials Science, Composite materials, Fracture mechanics, Materials Characterization & Testing, Properties and Mechanics, Nanomaterials, Aerospace and Automotive Engineering, and Structural Engineering\"-- Provided by publisher.
BOOK
Martensite Formation and Decomposition during Traditional and AM Processing of Two-Phase Titanium Alloys—An Overview
Titanium alloys have been considered as unique materials for many years. Even their microstructure and operational properties have been well known and described in details, the new technologies introduced—e.g., 3D printing—have restored the need for further research in this area. It is understood that martensitic transformation is usually applied in heat treatment of hardenable alloys (e.g., Fe alloys), but in the case of titanium alloys, it also occurs during the thermomechanical processing or advanced additive manufacturing. The paper summarizes previous knowledge on martensite formation and decomposition processes in two-phase titanium alloys. It emphasizes their important role in microstructure development during conventional and modern industrial processing.
Journal Article
An in situ synchrotron X-ray study of reverse austenitic transformation in a metastable FeMnCo alloy
This study concerns reverse austenitic transformation of plastic strain-induced hexagonal close-packed martensite. With the aid of in situ synchrotron X-ray diffractometry, the kinetic features of the transformation and the defect content evolution in a metastable (Fe
60
Mn
40
)
85
Co
15
alloy are quantitatively examined using 5, 20, and 100 °C/min heating rates. It is found that the reverse austenitic transformation can be activated below 200 °C and completes within a short time scale. Through a Kissinger-style kinetic analysis, the activation energy of the reverse austenitic transformation is determined as 171.38 kJ/mol, confirming its displacive nature. Although exponential attenuation is observed in both stacking fault probability and dislocation density upon the initiation of the transformation, the resulting microstructure (single-phase face-centered cubic structure) remains highly defected, exhibiting high Vickers hardness, but still preserving somewhat strain hardenability. Atomistic mechanisms for the reverse austenitic transformation are further conceived according to the crystallographic theory of martensitic transformation.
Graphical abstract
Journal Article
Microstructural Influence on Fracture Toughness of IF Steel and DP Steel
Interstitial free steels (IF) and Dual-phase (DP) steels are widely used in the automotive industry, their specific application is driven by requirements to optimize the strength-to-weight ratio. Utilizing the full capacity of their plasticity and strain hardenability requires an assessment of edge fracture susceptibility and flangeability. In this work, the ability of the mentioned steels to spreading of deformation along initiated cracks is evaluated by structural and fractographic analyzes. Microstructural restrictions of plasticity are correlated with fracture toughness results, adopting the essential work of fracture (EWF) methodology. Crystallographic analyzes (EBSD) are focused on the role of anisotropy and the deformation texture evolution, affecting the development of plasticity and thus the energy consumption to the fracture.
Journal Article
The Advancement of 7XXX Series Aluminum Alloys for Aircraft Structures: A Review
7XXX series aluminum alloys (Al 7XXX alloys) are widely used in bearing components, such as aircraft frame, spars and stringers, for their high specific strength, high specific stiffness, high toughness, excellent processing, and welding performance. Therefore, Al 7XXX alloys are the most important structural materials in aviation. In this present review, the development tendency and the main applications of Al 7XXX alloys for aircraft structures are introduced, and the existing problems are simply discussed. Also, the heat treatment processes for improving the properties are compared and analyzed. It is the most important measures that optimizing alloy composition and improving heat treatment process are to enhance the comprehensive properties of Al 7XXX alloys. Among the method, solid solution, quenching, and aging of Al 7XXX alloys are the most significant. We introduce the effects of the three methods on the properties, and forecast the development direction of the properties, compositions, and heat treatments and the solution to the corrosion prediction problem for the next generation of Al 7XXX alloys for aircraft structures. The next generation of Al 7XXX alloys should be higher strength, higher toughness, higher damage tolerance, higher hardenability, and better corrosion resistance. It is urgent requirements to develop or invent new heat treatment regime. We should construct a novel corrosion prediction model for Al 7XXX alloys via confirming the surface corrosion environments and selecting the accurate and reliable electrochemical measurements.
Journal Article
High strength and ductility combination in nano-/ultrafine-grained medium-Mn steel by tuning the stability of reverted austenite involving intercritical annealing
The structure–property relationship in 0.06C–5.5Mn steel subjected to different annealing temperatures and time was studied. Mn played a stronger effect on stabilizing austenite in comparison with Ni, and low-C medium-Mn steel possessed excellent hardenability. The reverse transformation of martensite to austenite occurred during intercritical annealing, and the volume fraction was first increased and then decreased on increasing annealing temperature or prolonging annealing time, indicative of change in thermal stability by element partitioning and coarsening of grain size. Correspondingly, the elongation was first increased and then decreased, consistent with the variation in the stability of reverted austenite. The yield strength was gradually decreased because of several factors, including recrystallization of α′ martensite, decreased stability of reverted austenite, and coarse grain size. The maximum product of strength and ductility was obtained on annealing at 650 °C for 10 min, which was attributed to the optimal stability of reverted austenite rather than the highest volume fraction, and tensile strength and elongation were 1120 MPa and 23.3%. The strain partitioning behavior of two phases was elucidated by analyzing Lüders straining and continuous work hardening after yield point elongation, and the deformation mechanism was strongly related to the stability of reverted austenite.
Journal Article
Recent Progress in Testing and Characterization of Hardenability of Aluminum Alloys: A Review
In this paper, the progress of the test methods and characterization approaches of aluminum alloys hardenability was reviewed in detail. The test method mainly included the traditional end-quenching method and the modified method. While the characterization approaches of alloy hardenability consist mainly of ageing hardness curves, solid solution conductivity curves, ageing tensile curves, time temperature transformation (TTT) curves, time temperature properties (TTP) curves, continuous cooling transformation (CCT) curves, and advanced theoretical derivation method have appeared in recent years. The hardenability testing equipment for different tested samples with different material natures, engineering applications properties, and measurement sizes was introduced. Meanwhile, the improvement programmed proposed for shortcomings in the traditional hardenability testing process and the current deficiencies during the overall hardenability testing process were also presented. In addition, the influence factors from the view of composition design applied to the hardenability behaviors of Aluminum alloys were summarized. Among them, the combined addition of micro-alloying elements is considered to be a better method for improving the hardenability of high-strength aluminum alloys.
Journal Article
Improving Hardenability Modeling: A Bayesian Optimization Approach to Tuning Hyperparameters for Neural Network Regression
This study investigates the application of regression neural networks, particularly the fitrnet model, in predicting the hardness of steels. The experiments involve extensive tuning of hyperparameters using Bayesian optimization and employ 5-fold and 10-fold cross-validation schemes. The trained models are rigorously evaluated, and their performances are compared using various metrics, such as mean square error (MSE), root mean square error (RMSE), mean absolute error (MAE), and coefficient of determination (R2). The results provide valuable insights into the models’ effectiveness and their ability to generalize to unseen data. In particular, Model 4208 (8-85-141-1) emerges as the top performer with an impressive RMSE of 1.0790 and an R2 of 0.9900. The model, which was trained with different datasets for nearly 40 steel grades, enables the prediction of hardenability curves, but is limited to the range of the training dataset. The research paper contains an illustrative example that demonstrates the practical application of the developed model in determining the hardenability band for a specific steel grade and shows the effectiveness of the model in predicting and optimizing heat treatment results.
Journal Article
Metastability in high-entropy alloys: A review
Classical alloy design strategies often aim to benefit from metastability. Examples are numerous: metastable transformation- and twinning-induced plasticity steels, cobalt or titanium based alloys, age hardenable aluminum alloys, and severe plastic deformed nanostructured copper. In each of these cases, superior engineering property combinations are achieved by exploring limits of stability. For the case of high-entropy alloys (HEAs), on the other hand, majority of present research efforts focus on exploring compositions that would yield stable single-phase structures. HEA metastability and its effects on microstructure and property development constitute only a relatively small fraction of ongoing work. To help motivate and guide a corresponding shift in HEA research efforts, here in this paper, we provide an overview of the research activities on metastability in HEAs. To this end, we categorize the past research on the topic into two groups based on their focus, namely, compositional and structural stability, and discuss the most relevant and exciting findings.
Journal Article
Individual Contribution of Zn and Ca on Age-Hardenability and Formability of Zn-Based Magnesium Alloy Sheet
This paper reports on the dilemma of the strength and forming behavior of magnesium alloy sheets due to hot rolling and precipitation aging as an obstacle for property adjustment. The effect of the Zn content on the age-hardenability and formability of Mg-Zn-Al-Ca-Mn sheets was investigated. Sheets of two alloys with 2 or 4 wt.% Zn, respectively, were produced by casting and subsequent hot rolling and their microstructure development, precipitation behavior and formability were examined. With higher Zn content the age-hardenability was increased, but at the same time the formability of the sheet decreased, concurrent to the basal-type texture development during rolling. On the other hand, the sheet containing a lower amount of Zn exhibited a weak rolling texture and rather high formability but low age-hardenability. The addition of a larger amount of Zn improved the age-hardenability through the formation of β1′ and β2′ phases. The basal texture was exhibited due to the consumption of solute Ca due to the formation of the Ca2Mg6Zn3 phase. This study suggests that this contradictory exhibition of the age-hardenability and formability of Ca-containing and Zn-based alloy sheets requires a strategical approach in alloy and process design, which allows tailoring the alloying elements and processing for the respective purpose.
Journal Article