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This study aims to investigate the sliding wear behavior of Al 0.4 FeCrNiCo x ( x = 0, 0.25, 0.5, 1.0 mol) high-entropy alloys (HEAs) under oil lubricating conditions at room temperature. Phase and microstructural characterizations of HEAs are performed by utilizing X-ray photoelectron spectroscopy (XRD) and scanning electron microscope (SEM). The compressive yield strength of Al 0.4 FeCrNiCo x ( x = 0, 0.25, 0.5, 1.0 mol) HEAs is observed to decrease from 1169.35 to 257.63 MPa. Plastic deformation up to 75% is achieved in the case of Al 0.4 FeCrNiCo x =1 HEA. The microhardness of HEA samples is found to decrease from 377 to 199 HV after the addition of cobalt content from x = 0 to 1.0 mol. Thermal analysis is performed using a differential scanning calorimeter. It is confirmed that Al 0.4 FeCrNiCo x ( x = 0, 0.25, 0.5, 1.0 mol) HEAs do not undergo any phase change up to 1000 °C. The specific wear rate of Al 0.4 FeCrNiCo x =1 HEA is observed to be highest in all wear conditions. The worn surfaces were analyzed by SEM with attached energy-dispersive spectroscopy, 3D profiling, and X-ray photoelectron spectroscopy (XPS).

A model is proposed that makes it possible to calculate the temperature dependence of the microhardness of glass over the entire temperature range from the softening temperature to absolute zero. The calculation uses the temperature dependence of the glass enthalpy and the value of its microhardness at the glass transition temperature. The proposed model is tested on the example of glassy selenium. For this, the temperature dependence of the microhardness of selenium on the softening temperature up to 100 K, which is 50 K below its Debye temperature, is measured. Thus, a relationship is established between the strength and thermodynamic properties of glass.

In the present research, a composite layer of TiO2-TiC-NbO-NbC was coated on the Ti-64 alloy using two different methods (i.e., the electric discharge coating (EDC) and electric discharge machining processes) while the Nb powder were mixed in dielectric fluid. The effect produced on the machined surfaces by both processes was reported. The influence of Nb-concentration along with the EDC key parameters (Ip and Ton) on the coated surface integrity such as surface topography, micro-cracks, coating layer thickness, coating deposition, micro-hardness has been evaluated as well. It has been noticed that in the EDC process the high peak current and high Nb-powder concentration allow improvement in the material migration, and a crack-free thick layer (215 μm) on the workpiece surface is deposited. The presence of various oxides and carbides on the coated surface further enhanced the mechanical properties, especially, the wear resistance, corrosion resistance and bioactivity. The surface hardness of the coated layer is increased from 365 HV to 1465 HV. Furthermore, the coated layer reveals a higher adhesion strength (~118 N), which permits to enhance the wear resistance of the Ti-64 alloy. This proposed technology allows modification of the mechanical properties and surface characteristics according to an orthopedic implant’s requirements.

The aim of this study was to assess the microhardness and surface roughness of bulk-fill resin composites treated with and without the application of an oxygen-inhibited layer (OIL) and a polishing system. This in vitro experimental study consisted of 72 resin composite blocks divided into three groups: Tetric N-Ceram Bulk Fill, Opus Bulk Fill APS, and Filtek Bulk Fill. Each resin composite group was further divided into two subgroups: with and without OIL control. Subsequently, surface roughness and microhardness were measured before and after polishing. A t-test was used to compare independent and related measures. For the intergroup comparison of variation before and after polishing, the Kruskal–Wallis test with Bonferroni post hoc was used considering a significance level of p < 0.05. When comparing surface roughness, significant differences were observed between Opus Bulk Fill resin composite with and without OIL control (p = 0.003) before polishing. The same occurred when comparing Tetric N-Ceram resin composite with and without OIL control (p = 0.039) after polishing. In addition, the surface roughness of Filtek Bulk Fill, Opus Bulk Fill, and Tetric N-Ceram Bulk Fill resin composites, with and without OIL control, decreased significantly after polishing (p < 0.001), while surface microhardness significantly increased (p < 0.05), with the exception of Opus Bulk Fill resin with OIL control (p = 0.413). In conclusion, OIL control and polishing significantly improved the surface roughness and surface microhardness of Filtek Bulk Fill and Tetric N-Ceram Bulk Fill resin composites. However, in the case of Opus Bulk Fill resin composite, only its surface roughness was significantly improved.

Polypropylene (PP) is an engineered thermoplastic polymer widely used in various applications. This work aims to enhance the properties of PP with the introduction of titanium dioxide (TiO2) nanoparticles (NPs) as nanofillers. Novel nanocomposite filaments were produced at 0.5, 1, 2, and 4 wt.% filler concentrations, following a melt mixing extrusion process. These filaments were then fed to a commercially available fused filament fabrication (FFF) 3D printer for the preparation of specimens, to be assessed for their mechanical, viscoelastic, physicochemical, and fractographic properties, according to international standards. Tensile, flexural, impact, and microhardness tests, as well as dynamic mechanical analysis (DMA), Raman, scanning electron microscopy (SEM), melt flow volume index (MVR), and atomic force microscopy (AFM), were conducted, to fully characterize the filler concentration effect on the 3D printed nanocomposite material properties. The results revealed an improvement in the nanocomposites properties, with the increase of the filler amount, while the microstructural effect and processability of the material was not significantly affected, which is important for the possible industrialization of the reported protocol. This work showed that PP/TiO2 can be a novel nanocomposite system in AM applications that the polymer industry can benefit from.

Laser metal deposition is a metal-based additive manufacturing technology. It is a very sensitive and complex process because of the different process parameters involved and the interrelations between these parameters. A thorough understanding of the underlying physics of the process is essential in developing a comprehensive database of the proper ties of materials processed with this technology. The main objective of this study was to investigate the effect of laser power on a laser-deposited 17-4 precipitation hardenable stainless steel alloy. The as-built microstructure, phase composition, microhardness and surface finish were analysed. The results show that a defect-free sample with good metallurgical bonding and minimal dilution can be produced using high laser power in the range 1400-2600 W and a scanning speed of 0.6 m/s. The microstructure in the clad layer was dominated by mar tensite and an improvement in surface finish and maximum hardness was observed with increased laser power.Significance: To fully benefit from the additive manufacturing technology, a comprehensive database of the material properties of alloys produced with this technology is required. This study expands on the body of knowledge related to the additive manufacturing of a 17-4PH stainless steel alloy, particularly highlighting the possibility of producing fully dense parts using higher laser power and scanning speed. These two parameters could significantly reduce the build time.

The microhardness and thickness of PVD coating layers made of titanium and hafnium nitrides were measured experimentally. The standards of TC 441 were analyzed. The sequence (protocol) of the analysis of nano-measurements and obtaining reliable measurement results was given. To obtain a quantitative value of the reliability of measurements for superhard nanocoats is proposed to use for educational purposes the calculation of the confidence interval using the Student criterion.

This research signifies an attempt to apply composite coating by co-deposition coating and assessing, enhancement the Nickel coatings features, by adding the particles of silicon-carbide to solution of electrodeposited. Stainless steel specimens have been subject to electroplating coating utilizing Nickel and nanosilicon carbide particles (70-100 nm) with various amounts (16, 24, 32 and 40) g/L. After coating, the specimens were tested by SEM, AFM, impeded in a solution with 3.5 percent NaCl to investigate the corrosion performance. Then testing the microhardness, and wear resistance. Results obtained from this work showed a great reduction in corrosion currents caused by adding of inert nanoparticles. These enhancements had been detected on all conducted tests for corrosion and wear.

A VC coating was prepared on the surface of mold steel Cr12MoV using the TD composite treatment process. The differences in microstructure and properties between the two composite treatment processes and the VC coating obtained from the ordinary TD vanadium infiltration process were compared using a microhardness tester, scratch tester, X-ray diffraction, etc. The results show that both composite processes can improve the unevenness of matrix carbides; The hardness of the VC coating obtained by the two composite processes is slightly higher than that of the ordinary TD; The TD+vacuum quenching process has to some extent improved the adhesion between the coating and the substrate; The valence state of the VC coating obtained by the secondary TD process has undergone significant changes.