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This study evaluated the influence of soil preparation method and initial moisture content on the compressive strength of cement-stabilized rammed earth (CSRE). Cube samples stabilized with 7–12% cement were compacted using a manual rammer, cured for up to 28 days, and tested according to adapted EN 12390-3 procedures. These results indicated that eliminating the powdering step improved laboratory efficiency and produced specimens more representative of field practice. These findings demonstrate that labor-intensive powdering of natural soils is unnecessary, provided that moisture is accurately determined, thereby improving both laboratory efficiency and consistency with field practice. The outcomes contribute to optimizing laboratory methodologies for earthen construction materials.

Our diet and its impact on the human gut microbiota in terms of composition and function are key determinants of human health across the life-course(1). Fermented vegetables can have enhanced functional and nutritional properties through substrate transformation by microbes and production of biochemicals during the fermentation process(2). Kimchi is a traditional Korean vegetable ferment produced via spontaneous lactic acid bacteria fermentation. Plant nutrients and biochemicals, microbial metabolites and microbial cell components are present in kimchi(3). As live products, fermented vegetables present challenges to commercial producers who need shelf/ transport stability to deliver consistent products to consumers. We hypothesise that fermented vegetable health advantages will be preserved by freeze-drying, while enabling product stability, extended shelf and storage life, stable transportation and utility as food ingredients. Utilising existing kimchi physiochemical data, we identified kimchi biochemicals (KBs) (benefit health but not essential to it) and kimchi nutrients (KNs) (essential to health). We quantified these components in 3-day old fresh kimchi (T3) and in 3-day old fresh kimchi that had been freeze-dried and powdered (T3 FDP). We sampled technical triplicates and calculated P values using an unpaired 2 tailed t-test. The hypothesis that KBs and KNs in T3 FDP are preserved at levels not statistically significantly different to those in (T3) (P > 0.005) was disproved. Components of kimchi were affected differently by the FDP process, with decreases in some and increases in others. As a result, the overall profile of KBs and KNs in T3 FDP was different to T3. Based on a daily portion of fresh kimchi being ∼50 g, there was 2.64 g KBs and KNs in 50 g T3 and 2.28 g KBs and KNs in equivalent portion T3 FDP (7.5 g), a reduction of 13.64% after FDP in KBs and KNs combined. Unexpectedly, soluble fibre and iron were significantly lower in equivalent sample T3 FDP compared to T3 (P = 0.003 and P < 0.0001 respectively) and vitamin B9 was significantly higher in T3 FDP compared to T3 (P < 0.0001). For KBs, acetic acid and lactic acid were significantly lower in T3 FDP (P = 0.020 and P = 0.046 respectively), but propionic acid was undetectable in T3 and the equivalent sample T3 FDP contained 1.44 g. Capsaicinoids were not detectable in T3, but were notably present in T3 FDP. This study represents a critical first step in understanding the extent to which the functionality of fresh kimchi is preserved in its freeze dried and powdered form (termed a FermentceuticalTM). Improving health through fermented foods is a critical concept for consumers, food manufacturers and healthcare professionals, alike.

In order to transform the crystalline form of Ca2SiO4 (C2S) in phosphorus-containing slag from monoclinic β-polycrystalline to square γ-polycrystalline, a volume expansion of about 11% was generated, which caused the phosphorus-containing slag to undergo self-powdering. The CaO-SiO2-Al2O3-MgO-MnO-P2O5-FeO slag system was analyzed using FactSage7.1 thermodynamic software, and the effects of different P2O5, FeO and basicity on the mineral phase composition of slag system were analyzed in the range of 1300~1700 °C. It was shown that P2O5, FeO and basicity all have an effect on the composition of the mineral phases. When the mass fraction of P2O5 in the slag was lower than 0.25%, it had less effect on the transformation of C2S crystalline structure. When the P2O5 content was higher than 0.25%, it was favorable to the generation of low-melting-point substances, but the P2O5 in the slag reacted with C2S in the silicate phase, making P5+ solidly soluble in C2S, inhibiting the transformation of β-C2S to γ-C2S and hindering the self-powdering of the slag. The FeO content in the slag system ranged from 20% to 28%, and as the FeO content increased, the C2S content in the silicate phase decreased from 33.3% to 25.9%, while the temperature at which the silicate was completely dissolved into the liquid phase decreased from 1600 °C to 1500 °C and the complete melting temperature of the slag decreased. The low FeO content facilitates the self-powdering of slag. In the high-phosphorus slag, at temperatures below 1450 °C, with the increase of basicity, the proportion of C2S in the silicate phase first increased and then decreased. With basicity at 1.8; the highest content of silicate phase, accounting for 33.7%; and the temperature exceeding 1450 °C, the silicate phase dissolved into the liquid phase, which is conducive to the removal of phosphorus from the slag, achieving the self-powdering of high-phosphorus slag.

This study evaluates the effectiveness of a small particle reagent (SPR) formulation based on Phloxine B dye for developing latent fingerprints on submerged non-porous surfaces. The primary objectives were to assess the formulation’s ability to produce fingerprints over time and determine its shelf life. The reagent was tested on three non-porous surfaces—glass, aluminium foil, and plastic transparency sheets—submerged in tap water for a duration of 30 days. Additionally, the study extended to evaluate the reagent’s performance on surfaces submerged in sewage water. The results demonstrated that the formulation successfully developed high quality identifiable fingerprints over a period of 27 days on glass, 29 days on transparency sheets, and 24 days on aluminium foil, after submersion in tap water. In the case of surfaces submerged in sewage water for 84 h, metal produced higher-quality and more durable prints compared to glass and plastic. On average, the Phloxine B-based SPR formulation demonstrated a shelf life of about 60 days. This Phloxine B-based SPR composition offers a non-toxic, cost-effective, and highly efficient approach, in the recovery of latent fingerprints from submerged non-porous surfaces.

This research studied the production of cricket powder via tray drying and powdering processes by investigating the effect of drying temperature of 80, 90, 100oC and drying time ranging of 30 - 240 min on the properties of cricket powder. The drying rate increased while the moisture content decreased as drying temperature and drying time increased causing it easy to be ground and had good solubility. The cricket powder had dark brown color and its lightness decreased with increasing drying temperature. The produced cricket powder could reach equilibrium moisture content of approximately 5% and the water activity was decreased with increasing drying temperature. Regarding the nutrient content, the change in drying temperature in a range of 80-100oC had no significant effect on the nutrient content. The suitable drying condition of crickets offering the highest protein content of 70.35% was achieved at drying temperature of 80oC and drying time of 240 min. At this condition, 55.57% yield of cricket powder satisfying dry food specification (moisture content of 5.32% and aw of 0.3539) was obtained.

Rosehip is of notable scientific interest due to its rich content of bioactives and its wide-ranging applications in nutrition, cosmetics and pharmaceuticals. The valorization of rosehip by-products, such as pomace, is highly significant for promoting sustainability. This study investigates the development of rosehip-based powders and beverage prototypes derived from both juice and pomace to evaluate the potential use of pomace in instant beverage design and compare it with juice-based formulations. Three matrices were evaluated: non-pasteurized and pasteurized juice, as well as non-pasteurized pomace preparations. Powders were produced by freeze- and spray drying using maltodextrin, inulin and unconventional carriers, i.e., palatinose and trehalose. The results demonstrated that carrier addition significantly influenced the physical and techno-functional properties of the powders, such as moisture content (below 10%), water activity (below 0.35), solubility (above 85%), and color indexes (yellowness and browning). The water absorption capacity varied with drying techniques, particularly for inulin-enriched samples, while the matrix type affected the ascorbic acid content. Non-pasteurized pomace powders exhibited a higher antioxidant capacity (67.7 mmol Trolox/100 g dry matter) than their juice counterparts (52.2 mmol Trolox/100 g dry matter), highlighting the potential of the pomace matrix for beverage production. Because of their favorable properties, spray-dried samples were also selected for reconstitution into prototype beverages, among which those obtained from pomace showed a higher antioxidant potential. An analysis of particle sizes, which ranged between 34 nm and 7363 nm, revealed potential interactions between the carrier and matrix, reflected in the distinct behavior of carrier-only samples. Both the carrier type and the matrix significantly contributed to the final properties of the beverages, providing valuable insights for the design of functional food products.

Silicone rubber insulation materials are widely used in energy systems. The powdering of silicone rubber sheds is a newly discovered aging phenomenon in recent years, and there is no specific research. In this paper, the powder composition of the composite insulators in coastal areas was studied, and the powdering process of silicone rubber under a high humidity environment of salt fog was repeated in the laboratory. The results show that the powders can be divided into two types according to particle shape, element composition, and molecule groups: the inorganic filler and its dehydrated product and the small molecule siloxane after polymer aging fracture. The particle size of Type I of powder is 3∼8μm, and the particle size of Type II of small molecule siloxane is 0.3∼1.1μm. The surface hydrophobicity of the powdered sample in a salt-fog environment will deteriorate, and the static contact angle will decrease. However, the hydrophobicity will gradually recover after leaving the harsh environment. Powdering of composite insulator silicone rubber in coastal areas is a complex physical and chemical process caused by the combined action of electricity, heat, and moisture. During this, polymer molecular chains break, and fillers gradually precipitate, forming powders.

•NIR powders were compared to conventional black and luminescent powders.•Black and GREENcharge™ powders are the most effective powders on the surfaces tested.•NIR powders do not offer significant advantage on conventional substrates.•Universal Powder outperformed fpNATURAL 1® in NIR luminescent conditions. Fingerprint powders remain one of the most common detection techniques used at the crime scene. However, powder efficiency and contrast can be hindered when applied to highly patterned backgrounds. This problem can be overcome using powders that are luminescent in the near-infrared (NIR) region of the electromagnetic spectrum. Despite being commercially available, those powders have been the focus of only a small number of studies, limited to a few substrates or donors. Their performance and advantages over common techniques are still to be thoroughly investigated. This study aims at assessing the performances of two NIR powder (fpNATURAL 1® and Universal Powder an in-house developed powder) against two conventional powders, a black and a luminescent powder (Sirchie Black, GREENcharge™) under various optical conditions (white light, visible luminescence and NIR luminescence). The powders were compared on four substrates using fingermarks of four different ages from five donors. A total 900 fingermarks were collected for each pairwise comparison. NIR imaging provided good background suppression and a high contrast, however it was shown that conventional powders remained the most effective powdering methods on the substrates tested as sufficient contrast could be achieved under white light or in luminescent mode in the visible region. The results showed that Universal Powder performed similarly to conventional powders, but poor performances were obtained on most substrates with fpNATURAL 1®. Based on the results obtained, it is recommended to use NIR powders only on substrates or conditions where traditional powders are known to perform poorly.

Skeletal remains are the only source of the genetic material of decomposed organisms or once-lived species. Unlike, soft tissues they are highly mineralized, and their anatomical and morphological structure prevents their deformation in the presence of adverse environmental factors. Therefore, bones and teeth protect the Deoxyribonucleic Acid (DNA) inside them. Obtaining DNA from hard tissues comes with challenges like contamination, degradation, PCR inhibitors, damage done by the environment on remains, etc. Traditional methods have been in use for a long time. To overcome the challenges in extracting DNA from hard tissues, researchers introduced various modifications, with time, to the standard procedures. We have reviewed the innovative approaches developed during the period ranging from 2000 to 2024, using the Google Scholar search engine. The last innovative method was discovered in 2021. Each method solves a particular challenge and makes it easier for future researchers to opt for a suitable protocol according to the specific requirements of their study. The methods were renamed based on their core specification, such as Carrier-Mediated Precipitation Method, CTAB Method, Buffered-Nondestructive Extraction Method, MDNAMI Method, Demineralization protocol, Rapid Column-based DNA Extraction, Bone Powdering and Bone Slicing, Short Fragmented DNA Extraction, Highly Degraded DNA Extraction, and Non-destructive Tooth DNA Extraction. A collaboration of researchers from forensic science, anthropology, archeology, evolutionary biology, molecular biology, etc. may develop more sophisticated techniques that ease extraction, increase yield, and reduce contamination of DNA from hard tissues. [Display omitted] •Hard tissues like skeletal remains are stable source of DNA because their structure protects them from degradation.•Challenges including contamination, environmental challenges and PCR inhibitors are faced during DNA extraction.•This study focuses on the recommendations to overcome these challenges of contamination and low yield.•Forensic anthropologists, archaeologist, and molecular biologists can ease these extraction techniques.

Paper cultural relics are prone to embrittlement, yellowing, powdering, mildew and damage due to the brittleness of materials, natural deterioration, microbial corrosion, and man-made destruction. To prolong the expected life of paper cultural relics, a series of novel microcrystalline cellulose/TiO2/fluorine/styrene-acrylate coatings were prepared with modified microcrystalline cellulose, modified nano-TiO2, dodecafluoroheptyl methacrylate, and several acrylate monomers. The prepared coatings were analyzed by infrared spectroscopy, transmission electron microscopy, UV–Vis spectroscopy, and performance-testing devices. In addition, the optimized protective coatings were coated on the simulated paper cultural relic surface, and its protective effects were evaluated by tensile strength retention rate and weight loss rate. When the content of modified nano-TiO2 was 1.0 wt%, the protective coatings exhibited good hydrophobicity, oil repellency, mechanical strength, anti-aging, and reversibility.Graphic abstract