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Magnesium alloys, renowned for their lightweight yet high-strength characteristics, with exceptional mechanical properties, are highly coveted for numerous applications. The emergence of magnesium alloy additive manufacturing (Mg AM) has further propelled their popularity, offering advantages such as unparalleled precision, swift production rates, enhanced design freedom, and optimized material utilization. This technology holds immense potential in fabricating intricate geometries, complex internal structures, and performance-tailored microstructures, enabling groundbreaking applications. In this paper, we delve into the core processes and pivotal influencing factors of the current techniques employed in Mg AM, including selective laser melting (SLM), electron beam melting (EBM), wire arc additive manufacturing (WAAM), binder jetting (BJ), friction stir additive manufacturing (FSAM), and indirect additive manufacturing (I-AM). Laser powder bed fusion (LPBF) excels in precision but is limited by a low deposition rate and chamber size; WAAM offers cost-effectiveness, high efficiency, and scalability for large components; BJ enables precise material deposition for customized parts with environmental benefits; FSAM achieves fine grain sizes, low defect rates, and potential for precision products; and I-AM boasts a high build rate and industrial adaptability but is less studied recently. This paper attempts to explore the possibilities and challenges for future research in AM. Among them, two issues are how to mix different AM applications and how to use the integration of Internet technologies, machine learning, and process modeling with AM, which are innovative breakthroughs in AM.

This book provides an updated state-of-the-art review on new developments in alkali-activation.The main binder of concrete, Portland cement, represents almost 80% of the total CO2 emissions of concrete which are about 6 to 7% of the Planet's total CO2 emissions.

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The emerging technology of wire arc additive manufacturing (WAAM) has been enthusiastically embraced in recent years mainly by the welding community to fabricate various grades of structural materials. In this study, ER70S-6 low-carbon low-alloy steel wall was manufactured by WAAM method, utilizing a gas metal arc welding (GMAW) torch translated by a six-axis robotic arm, and employing advanced surface tension transfer (STT) mode. The dominant microstructure of the fabricated part contained randomly oriented fine polygonal ferrite and a low-volume fraction of lamellar pearlite as the primary micro-constituents. Additionally, a small content of bainite and acicular ferrite were also detected along the melt-pool boundaries, where the material undergoes a faster cooling rate during solidification in comparison with the center of the melt pool. Mechanical properties of the part, studied at different orientations relative to the building direction, revealed a comparable tensile strength along the deposition (horizontal) direction and the building (vertical) direction of the fabricated part (~ 400 MPa and ~ 500 MPa for the yield and ultimate tensile strengths, respectively). However, the obtained plastic tensile strain at failure along the horizontal direction was nearly three times higher than that of the vertical direction, implying some extent of anisotropy in ductility. The reduced ductility of the part along the building direction was associated with the higher density of the interpass regions and the melt-pool boundaries in the vertical direction, containing heat-affected zones with coarser grain structure, brittle martensite–austenite constituent, and possibly a higher density of discontinuities.

The quality of powder used in powder bed-based additive manufacturing plays a key role concerning process performance and end part properties. Even though this is a generally accepted fact, there is still a lack of a comprehensive understanding of the powder property–part property relationship. However, numerous investigations focusing on selected powder properties and their corresponding influence on process aspects or final part properties have been published in recent years. Still, generalized statements on powder requirements for a defined process performance are not available. This can be attributed to the fact that the community has not yet come to an agreement which characterization techniques are most suitable for powder characterization in the additive manufacturing context and in most cases only selected aspects have been investigated for special powder materials. The aim of this review is to assess these building blocks of knowledge and to provide an overview on the current state of the art.

Wire + arc additive manufacturing (WAAM) is a versatile, low-cost, energy-efficient technology used in metal additive manufacturing. This WAAM process uses arc welding to melt a wire and form a three-dimensional (3D) object using a layer-by-layer stacking mechanism. In the present study, a Ni-based superalloy wire, i.e., Inconel 625, is melted and deposited additively through a cold metal transfer (CMT)-based WAAM process. The deposited specimens were heat-treated at 980 °C (the recommended temperature for stress-relief annealing) for 30, 60, and 120 min and then water quenched to investigate the effect of heat treatment on microstructure and phase transformation and to identify the optimum heat treatment condition. Microstructural results show that the heat treatment, in general, eliminates the brittle Laves phases regardless of the time without changing the grain morphology. However, an increment in the amount of the delta phase is observed with the longer heat treatment periods. Additionally, the size of MC (metal carbide) of Nb is also observed to increase with heat treatment time. This study provides an in-depth understanding of the correlation between heat treatment time and microstructure in additively manufactured Inconel 625, which can facilitate determining the optimum heat treatment condition in a later study.

Additive manufacturing, often known as three-dimensional (3D) printing, is a process in which a part is built layer-by-layer and is a promising approach for creating components close to their final (net) shape. This process is challenging the dominance of conventional manufacturing processes for products with high complexity and low material waste 1 . Titanium alloys made by additive manufacturing have been used in applications in various industries. However, the intrinsic high cooling rates and high thermal gradient of the fusion-based metal additive manufacturing process often leads to a very fine microstructure and a tendency towards almost exclusively columnar grains, particularly in titanium-based alloys 1 . (Columnar grains in additively manufactured titanium components can result in anisotropic mechanical properties and are therefore undesirable 2 .) Attempts to optimize the processing parameters of additive manufacturing have shown that it is difficult to alter the conditions to promote equiaxed growth of titanium grains 3 . In contrast with other common engineering alloys such as aluminium, there is no commercial grain refiner for titanium that is able to effectively refine the microstructure. To address this challenge, here we report on the development of titanium–copper alloys that have a high constitutional supercooling capacity as a result of partitioning of the alloying element during solidification, which can override the negative effect of a high thermal gradient in the laser-melted region during additive manufacturing. Without any special process control or additional treatment, our as-printed titanium–copper alloy specimens have a fully equiaxed fine-grained microstructure. They also display promising mechanical properties, such as high yield strength and uniform elongation, compared to conventional alloys under similar processing conditions, owing to the formation of an ultrafine eutectoid microstructure that appears as a result of exploiting the high cooling rates and multiple thermal cycles of the manufacturing process. We anticipate that this approach will be applicable to other eutectoid-forming alloy systems, and that it will have applications in the aerospace and biomedical industries. Titanium–copper alloys with fully equiaxed grains and a fine microstructure are realized via an additive manufacturing process that exploits high cooling rates and multiple thermal cycles.

Invar 36 has gained considerable popularity in many industries, including the aerospace industry, because of its low coefficient of thermal expansion. In this paper, a brief overview for the research needs in metal additive manufacturing is presented. A thorough study for the influence of process parameters on the quality of the parts produced is presented. This study is beneficial for the long-term growth of the additive manufacturing industry. The paper aims to select the process parameters that can be used to fabricate dense parts from Invar 36 ( UNS K93600 ) using the selective laser melting process. In this research, a group of cubes was fabricated using different process parameters from Invar 36 powder using a selective laser melting machine. The density, microstructures, and surface features of these cubes were measured. Experimental observations were drawn from the results of the preliminary analyses. The influence of the process parameters on the density of the parts produced is discussed in this paper.

Titanium alloys are expensive and difficult to process into large complex components for aerospace applications. Directed energy deposition (DED), one of the additive manufacturing (AM) technologies, offers a high deposition rate, being suitable for fabricating large metallic components. So far, most review articles on the AM of titanium discuss the popular powder bed fusion method with the emphasis on the “workhorse” titanium alloy—Ti-6Al-4V. There have been few review articles on the DED process of a broad range of titanium alloys—near-α, β, and other α + β alloys beyond Ti-6Al-4V. This article focuses on the processing–microstructure–property relationships in the DED-processed titanium alloys (Ti-6Al-4V and beyond) with the following aspects: (1) microstructure evolution induced by solidification, thermal cycles, and post-processing heat treatment; (2) tensile properties of as-deposited and heat-treated titanium alloys; (3) defects, residual stresses, and fatigue properties; and (4) micro/nanomechanical properties. The article concludes with perspectives about future directions in this field.

Aluminum alloys are in high demand for additive manufacturing (AM) processing. However, the physical properties of Al alloys are less favorable for the production of repeatable and reliable parts, with factors such as surface oxide scales, high thermal conductivity, and large solidification shrinkage. Despite these characteristics, processing strategies have been developed to overcome these hurdles. The objective of this article is to highlight the different microstructure–processing–properties characteristics for the three main families of aluminum alloys: pure, casting, and wrought chemistries. The article focuses on AM processes involving solidification, including powder bed and direct energy deposition for both powder and wire feedstock.