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Agglomeration, colloidal stability, and magnetic separation of magnetic nanoparticles: collective influences on environmental engineering applications
Magnetic nanoparticles (MNPs) which exhibit magnetic and catalytic bifunctionalities have been widely accepted as one of the most promising nanoagents used in water purification processes. However, due to the magnetic dipole-dipole interaction, MNPs can easily lose their colloidal stability and tend to agglomerate. Thus, it is necessary to enhance their colloidal stability in order to maintain the desired high specific surface area. Meanwhile, in order to successfully utilize MNPs for environmental engineering applications, an effective magnetic separation technology has to be developed. This step is to ensure the MNPs that have been used for pollutant removal can be fully reharvested back. Unfortunately, it was recently highlighted that there exists a conflicting role between colloidal stability and magnetic separability of the MNPs, whereby the more colloidally stable the particle is, the harder for it to be magnetically separated. In other words, attaining a win-win scenario in which the MNPs possess both good colloidal stability and fast magnetic separation rate becomes challenging. Such phenomenon has to be thoroughly understood as the colloidal stability and the magnetic separability of MNPs play a pivotal role on affecting their effective implementation in water purification processes. Accordingly, it is the aim of this paper to provide reviews on (i) the colloidal stability and (ii) the magnetic separation of MNPs, as well as to provide insights on (iii) their conflicting relationship based on recent research findings.
Graphical abstract
Interrelationship of agglomeration, colloidal stability, and magnetic separability of nanoparticles
Journal Article
Advanced oxidation technologies : sustainable solutions for environmental treatments
Providing a state-of-the-art overview on environmental applications of Advanced Oxidation Technologies (AOTs) as sustainable, low-cost and low-energy consuming treatments of water, air, and soil. It includes information on innovative research and development on TiO2 photocatalytic redox processes, Fenton, Photo-Fenton processes, zerovalent iron technology, etc highlighting possible applications of ATOs in developing and industrialized countries around the world in the framework of 'A crosscutting and comprehensive look at environmental problems'.
Book
Recent Advances in Ternary Metal Oxides Modified by N Atom for Photocatalysis
Ternary metal oxides (TMOs) with flexible band structures are of significant potential in the field of photocatalysis. The efficient utilization of renewable and green solar energy is of great importance to developing photocatalysts. To date, a wide range of TMOs systems has been developed as photocatalysts for water and air purification, but their practical applications in visible light-assisted chemical reactions are hindered mainly by its poor visible light absorption capacity. Introduction of N atoms into TMOs can narrow the band-gap energy to a lower value, enhance the absorption of visible light and suppress the recombination rate of photogenerated electrons and holes, thus improving the photocatalytic performance. This review summarizes the recent research on N-modified TMOs, including the influence of N doping amounts, N doping sites, and N-induced phase transformation. The introduced N greatly tuned the optical properties, electronic structure, and photocatalytic activity of the TMOs. The optimal N concentration and the influence of N doping sites are investigated. The substitutional N and interstitial N contributed differently to the band gap and electron transport. The introduced N can tune the vacancies in TMOs due to the charge compensation, which is vital for inducing different activity and selectivity. The topochemical ammonolysis process can convert TMOs to oxynitride with visible light absorption. By altering the band structures, these oxynitride materials showed enhanced photocatalytic activity. This review provides an overview of recent advances in N-doped TMOs and oxynitrides derived from TMOs as photocatalysts for environmental applications, as well as some relevant pointers for future burgeoning research development.
Journal Article
Solar photocatalysis for environmental remediation
The book presents a review of research and pilot-scale efforts undertaken by scientists all over the world towards utilization of solar energy for environmental remediation. It gives a complete account of the solar photocatalytic degradation of pollutants present in wastewater and atmosphere and also discusses the solid-phase photocatalytic degradation of plastics in the form of composite. The text further describes the hydrogen generation by photocatalytic water splitting. Various solar collectors and reactors used especially for environmental remediation are also elucidated.
Book
Functionalized Graphitic Carbon Nitrides for Environmental and Sensing Applications
Graphitic carbon nitride (g‐C3N4) is a metal‐free semiconductor that has been widely regarded as a promising candidate for sustainable energy production or storage. In recent years, g‐C3N4 has become the center of attention by virtue of its impressive properties, such as being inexpensive, easily fabricable, nontoxic, highly stable, and environment friendly. Herein, the recent research developments related to g‐C3N4 are outlined, which sheds light on its future prospective. Various synthetic methods and their impact on the properties of g‐C3N4 are detailed, along with discussion on frequently used characterization methods. Different approaches for g‐C3N4 surface functionalization, mainly categorized under covalent and noncovalent strategies, are outlined. Moreover, the processing methods of g‐C3N4, such as g‐C3N4‐based thin films, hierarchical, and hybrid structures, are explored. Next, compared with the extensively studied energy‐related applications of the modified g‐C3N4s, relatively less‐examined areas, such as environmental and sensing, are presented. By highlighting the strong potential of these materials and the existing research gaps, new researchers are encouraged to produce functional g‐C3N4‐based materials using diverse surface modification and processing routes. Fine‐tuning the physicochemical and electronic properties of graphitic carbon nitride (g‐C3N4) for the target applications has attracted much attention. This perspective details various covalent and noncovalent surface modifications of g‐C3N4. A brief discussion of synthetic routes, processing, and characterization methods used is also presented. Moreover, a section sheds light on the applications of functionalized g‐C3N4s in environmental monitoring and sensing.
Journal Article
Nanomaterials for environmental applications
\"The book offers a comprehensive review of the latest advances in nanomaterials-based technologies for the treatment of emerging contaminants in wastewater. It describes the latest developments in synthesis protocols, including synthesis of different kinds of nanostructure materials using various physical and chemical methods. Aimed at researchers and industry professionals, this work will be of interest to chemical, environmental, and materials engineered concerned with the application of advanced materials for environmental and water remediation\"-- Provided by publisher.
Book
Hydrogen Production as a Clean Energy Carrier through Heterojunction Semiconductors for Environmental Remediation
Today, as a result of the advancement of technology and increasing environmental problems, the need for clean energy has considerably increased. In this regard, hydrogen, which is a clean and sustainable energy carrier with high energy density, is among the well-regarded and effective means to deliver and store energy, and can also be used for environmental remediation purposes. Renewable hydrogen energy carriers can successfully substitute fossil fuels and decrease carbon dioxide (CO2) emissions and reduce the rate of global warming. Hydrogen generation from sustainable solar energy and water sources is an environmentally friendly resolution for growing global energy demands. Among various solar hydrogen production routes, semiconductor-based photocatalysis seems a promising scheme that is mainly performed using two kinds of homogeneous and heterogeneous methods, of which the latter is more advantageous. During semiconductor-based heterogeneous photocatalysis, a solid material is stimulated by exposure to light and generates an electron–hole pair that subsequently takes part in redox reactions leading to hydrogen production. This review paper tries to thoroughly introduce and discuss various semiconductor-based photocatalysis processes for environmental remediation with a specific focus on heterojunction semiconductors with the hope that it will pave the way for new designs with higher performance to protect the environment.
Journal Article
Efficient Activation of Persulfate by TiO2/g-C3N4 Composite for Degradation of Acetaminophen Under Visible Light
The massive use of acetaminophen (APAP) poses a potential crisis for humans and the environment. In this paper, the degradation of APAP in aqueous solution was carried out using photocatalytic synergistic persulfate oxidation. To enhance the photocatalytic activity of g-C3N4 and thus activate the persulfate (K2S2O8, PS) more effectively, the heterojunction photocatalyst TiO2/g-C3N4 (TCN) was prepared by a hydrothermal method. The TCN-PS catalytic system showed a high efficiency for APAP degradation. When the amount of TCN and PS added was 0.6 g/L, the degradation rate of APAP at 10 mg/L was 78.3% after 60 min of illumination. Moreover, the TCN-PS catalytic system was effective in removing organic pollutants in acidic, neutral, and weakly alkaline environments. The radical quenching experiment results indicate that both sulfate radicals (SO4−•) and hydroxyl radicals (•OH) are involved in the degradation reaction. After five cycles, the TCN-PS catalytic system still has stable catalytic activity.
Journal Article