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Research background. The worldwide demand for healthy and sulphur-free dried vegetables and fruits has grown. Combined ultrasound-assisted osmotic dehydration (UOD) and application of active coatings incorporating natural preservatives represents an attractive alternative for sulphuring process to preserve the sensorial and nutritional quality of dried fruits. The aim of this study was to investigate the effect of osmotic dehydration (OD) and UOD and the use of pectin coatings (alone or with citric acid, CA or ascorbic acid, AA) on physical, textural and microstructural properties of hot air-dried apricot. Experimental approach. Fresh apricot cubes (1 cm3) were pre-treated with either OD at a temperature of 55 °C for 30 and 45 min or UOD at two ultrasonic frequencies of 25 and 35 kHz for 30 and 45 min followed by application of active coatings with pectin alone, pectin + CA or pectin + AA for 10 min. All pre-treated coated samples were then hot-air dried at a temperature of 60 °C until a final moisture content of 20 % (wet basis) was reached. Physical (shrinkage, apparent and bulk densities), chemical (browning value, water activity), textural (firmness and shrinkage), microstructure and microbial load of dried apricot was studied. Results and conclusions. Application of OD and UOD improved physical and textural properties of the dried apricots. Moreover, apparent and bulk densities, rehydration capacity of OD and UOD pre-treated samples were increased. While, shrinkage, water activity and microbial load were decreased. Firmness of UOD pre-treated samples was significantly (p < 0.05) lower than that of OD ones. Likewise, increasing ultrasound frequency from 25 to 35 kHz led to a significant decrease in Fmax values of dried apricots. Furthermore, coating of the OD and UOD processed samples with pectin + CA increased Fmax and decreased rehydration capacity of dried apricots. Scanning electron microscopy of both OD and UOD samples illustrated improvement of textural properties. The utilization of both OD pre-treatment and pectin edible coatings resulted in a decrease in browning values. However, UOD increased browning values of the dried apricots. Coating of UOD samples with pectin + AA resulted in substantial discoloration in hot air-dried apricot. Novelty and scientific contribution. This study advances the knowledge in the field of fruit drying by combined application of OD or UOD pre-treatments with post-treatments with active edible coatings on different properties of hot-air dried apricot.

Tender coconut water has been very popular as a natural beverage rich in various electrolytes, amino acids, and vitamins, and hence a large amount of tender coconut kernel is left without efficient utilization. To explore the possibility of making infused tender coconut kernel, we investigated the effects of two osmosis methods, including solid-state osmotic dehydration and liquid-state osmotic dehydration, as well as two osmosis agents such as sorbitol and sucrose, on the mass transfer of coconut kernel under solid-state osmotic dehydration conditions. The results showed that under the conditions of solid-state osmosis using sucrose and liquid-state osmosis using sucrose solution, the water diffusion coefficients were 9.0396 h−1/2 and 2.9940 h−1/2, respectively, with corresponding water mass transfer coefficients of 0.3373 and 0.2452, and the equilibrium water loss rates of 49.04% and 17.31%, respectively, indicating that the mass transfer efficiency of solid-state osmotic dehydration of tender coconut kernel was significantly higher than that of liquid-state osmotic dehydration. Under solid osmosis conditions, the water loss rates using sucrose and sorbitol were 38.64% and 41.95%, respectively, with dry basis yield increments of 61.38% and 71.09%, respectively, demonstrating superior dehydration efficiency of sorbitol over sucrose under solid-state osmosis. This study can provide a reference for the theoretical study of the mass transfer of tender coconut kernel through osmotic dehydration, and also provide technical support for the development and utilization of tender coconut kernel.

Using frozen mango for osmotic hot air drying is still uncommon due to a lack of knowledge on the effect of the freezing process on the final product’s quality attributes. This study aimed to investigate the effect of the freezing method (slow and quick freezing) and frozen storage time at −18 °C (0, 1, and 2 months) on mass transfer kinetics during osmotic dehydration, drying kinetics during hot air drying, and final quality attributes of the dried mango. The results indicated that Peleg’s model could describe the water loss and solid gain during the osmotic dehydration in a 38° Brix sugar solution. Freezing before osmotic dehydration reduced the water loss rate while increasing the solid uptake content. Frozen mangoes showed slightly higher drying rates at 50 and 60 °C than the fresh ones. Freezing and frozen storage also retarded the browning reaction and polyphenol oxidase activities. The osmotic-dried mango obtained from frozen mangoes showed a chewy and gummy texture, which could be considered a distinctive texture characteristic for dried mango.

Tomato is one of the most cultivated vegetables, playing important role in the human feed. Due to its characteristics and composition, tomatoes present reduced shelf life, and preservative techniques are required. In this study, response surface methodology was used to optimize process conditions during the osmotic dehydration (OD) of tomato slices, through the desirability function. Optimization factors were absolute pressure (21-89 kPa), vacuum application period (7-15 min), and osmotic solution water activity (0.893-0.943), while investigated responses were sodium incorporation (NaI), water loss (WL), solid gain (SG), weight reduction (WR), and osmodehydrated product water activity (ODaw). The optimized conditions were achieved, and a further hot-air drying (HAD) was conducted at different temperatures and air velocities. During the OD, lower absolute pressure, and osmotic solution water activity led to lower NaI and higher WL and WR. Shorter drying time and higher diffusivity were obtained at higher temperature and air velocity, during the HAD. The dried tomato slices with sodium incorporation reduction were evaluated with regard to the final water activity, rehydration and color, in which no significant differences (p > 0.05) were observed between the treatments.

The knowledge about thermophysical properties of foods is especially important in thermal processing, influencing the design, optimization and cost reduction of the process, as well as the quality and safety of the final product. This article deals with the determination of some thermophysical properties of yacon, namely, specific mass, specific heat, thermal conductivity and thermal diffusivity during the osmo-convective drying. Yacon is a root with approximately 90% w.b. of moisture content, whose high concentration of fructooligosacharydes and antioxidants has gained attention in the food research field. Yacon slices were osmotically dehydrated for 2 hours in a sucralose solution and then dried in a convective tray dryer for 2 hours, varying the osmotic solutions temperature and stirring rate and temperature of the drying air. All thermophysical properties were determined during the drying process at 30-minute intervals. The thermophysical properties were determined not only experimentally but also calculated by models available in literature based on the products centesimal composition. A satisfactory agreement between experimental and predicted results was obtained. Further, empirical models obtained by nonlinear regression were successfully fitted to the experimental data, as a function of moisture content, within a 94% - 3% w.b. range.

Osmotic dehydration of fruits and vegetables is a slow process due to resistance in mass transfer (MT). This resistance can be modified by varying the osmotic solution or process conditions, or by employing non-thermal treatments (NTT). Some NTT modify the tissue structure by formation of pores in the cell membrane (such as pulse electric fields) or microchannels (such as ultrasound and osmosonication), and others increase the contact surface area with the tissue through a decrease in atmospheric pressure (such as vacuum pulses) or an increase of the system pressure (such as high hydrostatic pressures). Changes in the rate of MT caused by modifications in experimental conditions can be described with mathematical models, such as Fick’s second law. The aims of this review are to analyze the different factors that modify MT rate during osmotic dehydration, examine the application of NTT to modify MT, and to study models that describe these processes.

The aim of this study was to compare the effectiveness of microwave-vacuum pretreatment conducted at 100, 500 and 800 W on the drying kinetics of whole cranberries ( Vaccinium macrocarpon ) during hybrid osmotic and microwave-vacuum drying. Additionally, the effect of microwave-vacuum pretreatment and subsequent osmo-microwave-vacuum drying on selected quality indicators of dried cranberries, including phenolic content, antioxidant activity and color, was studied, and the quality of samples was compared with freeze dried, microwave-vacuum dried and osmo-microwave-vacuum dried samples. Irrespective of microwave power, the initial pretreatment accelerated mass transfer during osmotic dehydration of cranberries, and the Weibull model well fitted the experimental data. Final microwave-vacuum drying of cranberries was a two-stage process involving a relatively long phase with a constant drying rate, followed by a short period with a decreasing drying rate. Microwave-vacuum and osmo-microwave-vacuum drying resulted in similar retention of polyphenols and similar antioxidant activity, both of which were relatively higher than in freeze-dried cranberries. However, microwave-vacuum pretreatment at low microwave power (100 W) before dehydration also resulted in high retention of phenolic compounds, high antioxidant activity and attractive color, which were consistent with the high content of total anthocyanins and flavonoids. Microwave-vacuum, osmo-microwave-vacuum and osmo-microwave-vacuum drying combined with microwave-vacuum pretreatment at low microwave power (100 W) were the most suitable methods for the production of high-quality dried whole cranberries.

The main cause of perishability of fruits and vegetables are their high water content. To increase the shelf life of these fruits and vegetables many methods or combination of methods had been tried. Osmotic dehydration is one of the best and suitable method to increase the shelf life of fruits and vegetables. This process is preferred over others due to their vitamin and minerals, color, flavor and taste retention property. In this review different methods, treatments, optimization and effects of osmotic dehydration have been reviewed. Studied showed that combination of different osmotic agents were more effective than sucrose alone due to combination of properties of solutes. During the experiments it was found that optimum osmosis was found at approximately 40 °C, 40 °B of osmotic agent and in near about 132 min. Pretreatments also leads to increase the osmotic process in fruits and vegetables. Mass transfer kinetics study is an important parameter to study osmosis. Solids diffusivity were found in wide range (5.09–32.77 kl/mol) studied by Fick’s laws of diffusion. These values vary depending upon types of fruits and vegetables and osmotic agents.

This study summarizes the most recent findings on osmotic dehydration, a crucial step in food preservation. The many benefits of osmotic dehydration are listed, including longer shelf life and preserved nutritional value. Mass transfer dynamics, which are critical to understanding osmotic dehydration, are explored alongside mathematical models essential for comprehending this process. The effect of osmotic agents and process parameters on efficacy, such as temperature, agitation and osmotic agent concentration, is closely examined. Pre-treatment techniques are emphasized in order to improve process effectiveness and product quality. The increasing demand for sustainability is a critical factor driving research into eco-friendly osmotic agents, waste valorization, and energy-efficient methods. The review also provides practical insights into process optimization and discusses the energy consumption and viability of osmotic dehydration compared to other drying methods. Future applications and improvements are highlighted, making it an invaluable tool for the food industry.

The study investigated the effect of osmotic treatment, edible coatings, and reduced pressure on the quality of carrots dried by the microwave–vacuum method (MVD) at 3.5 or 6.5 kPa and microwave power of 250 W. Initial osmotic enrichment (OE) of carrots was carried out in chokeberry NFC juice, and osmotic dehydration (OD) in chokeberry juice concentrate. Coatings were prepared using sodium alginate or citrus pectin solutions of 1.0 or 1.5%. Osmotic treatment, and then drying pressure, had the greatest effect on increasing the dry matter (DM), total phenolic content (TPC), and color changes, but also on decreasing the water activity (AW) of dried carrot. The highest DM (average 98.7%) and the lowest AW (average 0.25) were obtained in OE carrots and dried at 3.5 kPa. Drying carrots, combined with osmotic treatment and coating, increased TPC by 13-fold, from 225 in fresh to 3229 mg GAE/100 g d.m. in dried carrots. Osmotic treatment did not affect the antioxidant activity of DPPH•, but OD significantly increased ABTS•+ compared to the raw material. Coatings had a smaller effect on color changes and antioxidant activity (DPPH• and ABTS•+) and no significant impact on DM and AW. The color changes of the control and coated samples were an increase in color lightness, redness, yellowness, and saturation (vividness), and those subjected to osmotic treatment showed a decrease in these parameters. The lower AW of dried carrots positively affected higher hardness. All samples were sensory accepted, including color, texture, and smell, especially after OD in chokeberry juice concentrate, while crunchiness was the lowest (five out of nine points).