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Formation of chromium-alloyed cementite in the process of mechanosynthesis and subsequent annealings
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Formation of chromium-alloyed cementite in the process of mechanosynthesis and subsequent annealings
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Journal Article
Formation of chromium-alloyed cementite in the process of mechanosynthesis and subsequent annealings
2015
Overview
Mössbauer spectroscopy and magnetic measurements have been used to investigate the formation of phases in the process of mechanosynthesis of a nanocomposite of composition (Fe
0.93
Cr
0.07
)
75
C
25
in a planetary ball mill with the subsequent annealings at various temperatures. It has been shown that, at the initial stage of the mechanosynthesis, an amorphous Fe-C phase is formed. Later, an amorphous Fe-Cr-C phase is formed and, in the process of the subsequent mechanosynthesis, an alloyed cementite is formed from it. It has been found that, due to the products of the pickup from the milling balls made of ShKh15 steel, the changes in the initial composition (Fe
0.93
Cr
0.07
)
75
C
25
of the powders that reach 5 wt % have almost no effect on the phase composition, specific saturation magnetization, and the coercive force of samples annealed at 800°C for 1 h.
Publisher
Pleiades Publishing,Springer,Springer Nature B.V
Subject
