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Synthesis and characterization of a cross-linking monomer based on 1,3-diallyl-1,3-dibicyclo4.2.0octa-1,3,5-trien-3-yl-1,3-dimethyl-siloxane

by Demin, D U , Chudov, K A , Lyssenko, K A , Kalashnikov, A Yu , Adamov, E G , Bulanova, A V , Grebennikov, E P , Levchenko, K S , Shmelin, P S

in Copolymers / Crosslinking / Dielectric properties / Monomers / Physical properties / Physics / Ring opening / Siloxanes / Thermal stability

2019

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Synthesis and characterization of a cross-linking monomer based on 1,3-diallyl-1,3-dibicyclo4.2.0octa-1,3,5-trien-3-yl-1,3-dimethyl-siloxane

by Demin, D U , Chudov, K A , Lyssenko, K A , Kalashnikov, A Yu , Adamov, E G , Bulanova, A V , Grebennikov, E P , Levchenko, K S , Shmelin, P S

in Copolymers / Crosslinking / Dielectric properties / Monomers / Physical properties / Physics / Ring opening / Siloxanes / Thermal stability

2019

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Synthesis and characterization of a cross-linking monomer based on 1,3-diallyl-1,3-dibicyclo4.2.0octa-1,3,5-trien-3-yl-1,3-dimethyl-siloxane

by Demin, D U , Chudov, K A , Lyssenko, K A , Kalashnikov, A Yu , Adamov, E G , Bulanova, A V , Grebennikov, E P , Levchenko, K S , Shmelin, P S

in Copolymers / Crosslinking / Dielectric properties / Monomers / Physical properties / Physics / Ring opening / Siloxanes / Thermal stability

2019

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Journal Article

Synthesis and characterization of a cross-linking monomer based on 1,3-diallyl-1,3-dibicyclo4.2.0octa-1,3,5-trien-3-yl-1,3-dimethyl-siloxane

Demin, D U,

Chudov, K A,

Lyssenko, K A,

Kalashnikov, A Yu,

Adamov, E G,

Bulanova, A V,

Grebennikov, E P,

Levchenko, K S,

Shmelin, P S

2019

Overview

New cross-linking monomer based on 1,3-diallyl-1,3-di[bicyclo[4.2.0]octa-1,3,5-trien-3-yl]-1,3-dimethyl-siloxane (BCB-All) was synthesized and its physical properties were studied. BCB-All was incorporated into copolymer with TGM-3 and PFHDA by two stage thermal polymerization. The cross-linking of the copolymers occurs by thermo-initiated ring-opening reaction of BCB at 120-200°C. Resulting BCB-All homopolymer, BCB-All-TGM-3 (50:50), and BCB-All-PFHDA (50:50) copolymers have high thermal stability (Td5%,=464°C, 322°C, 435°C respectively) and good dielectric properties (ε=2.34-2.48 at 10HHz).

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Publisher

IOP Publishing

Subject

Copolymers

/ Crosslinking

/ Dielectric properties

/ Monomers

/ Physical properties

/ Physics

/ Ring opening