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Synthesis, spectral characterization, and structural investigation of mononuclear salen-type Cu(II) and Zn(II) complexes of a potentially octadentate N2O6 Schiff base ligand derived from binaphthol
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Synthesis, spectral characterization, and structural investigation of mononuclear salen-type Cu(II) and Zn(II) complexes of a potentially octadentate N2O6 Schiff base ligand derived from binaphthol
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Synthesis, spectral characterization, and structural investigation of mononuclear salen-type Cu(II) and Zn(II) complexes of a potentially octadentate N2O6 Schiff base ligand derived from binaphthol
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Journal Article
Synthesis, spectral characterization, and structural investigation of mononuclear salen-type Cu(II) and Zn(II) complexes of a potentially octadentate N2O6 Schiff base ligand derived from binaphthol
2013
Overview
A new potentially octadentate N
2
O
6
Schiff base ligand, H
2
L derived from the condensation of 2,2′-(1,1′-binaphthyl-2,2′-diylbis(oxy))dianiline and o-vanillin, along with its copper(II) and zinc(II) complexes, is synthesized and has been characterized by elemental analyses, IR, UV–vis,
1
H and
13
C NMR spectra, as well as conductivity measurements. H
2
L forms mononuclear complexes of 1:1 (metal:ligand) stoichiometry with Cu(II) and Zn(II), and conductivity data confirm the non-electrolyte nature of these complexes. The [ZnL] and [CuL] complexes display very different solid-state structures, as determined by X-ray crystallography. While the [ZnL] complex has a distorted octahedral geometry about the metal, the [CuL] complex displays a distorted square planar geometry about the copper, with long Cu–O(ether) distances of 2.667 Å.
Publisher
Springer Netherlands
