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Surface Modification of Sodium Montmorillonite Nanoclay by Plasma Polymerization and Its Effect on the Properties of Polystyrene Nanocomposites

by Ibarra-Alonso, María Cristina , Soria-Arguello, Gustavo , Mora-Cortes, Luis Fernando , Hernández-Hernández, Ernesto , Castañeda-Facio, Adali Oliva , Velázquez, María Guadalupe Neira , Reyes-Acosta, Yadira Karina , Borjas-Ramos, José Javier , Narro-Céspedes, Rosa Idalia

in Carbon fibers / Clay / Composite materials / Emulsion polymerization / Fourier transforms / Infrared analysis / Investigations / Mechanical properties / Modulus of elasticity / Montmorillonite / Nanocomposites / Nanomaterials / Nanoparticles / Oxidation / Plasma / Polymerization / Polymers / Polymethyl methacrylate / Polystyrene resins / Scanning electron microscopy / Sodium / Thermodynamic properties / Thermogravimetric analysis / X-ray diffraction

2018

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Surface Modification of Sodium Montmorillonite Nanoclay by Plasma Polymerization and Its Effect on the Properties of Polystyrene Nanocomposites

2018

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Surface Modification of Sodium Montmorillonite Nanoclay by Plasma Polymerization and Its Effect on the Properties of Polystyrene Nanocomposites

2018

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Journal Article

Surface Modification of Sodium Montmorillonite Nanoclay by Plasma Polymerization and Its Effect on the Properties of Polystyrene Nanocomposites

Ibarra-Alonso, María Cristina,

Soria-Arguello, Gustavo,

Mora-Cortes, Luis Fernando,

Hernández-Hernández, Ernesto,

Castañeda-Facio, Adali Oliva,

Velázquez, María Guadalupe Neira,

Reyes-Acosta, Yadira Karina,

Borjas-Ramos, José Javier,

Narro-Céspedes, Rosa Idalia

2018

Overview

Sodium montmorillonite nanoclay (Na+-MMT) was modified by plasma polymerization with methyl methacrylate (MMA) and styrene (St) as monomers and was denominated as Na+-MMT/MMA and Na+-MMT/St, respectively. This plasma modified nanoclay was used as reinforcement for polystyrene (PS) nanocomposites that were prepared by melt mixing. Pristine and modified Na+-MMT nanoclay were analyzed by the dispersion in various solvents, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM). The results confirmed a change in hydrophilicity of the modified Na+-MMT, as well as the presence of a polymeric material over its surface. The pristine PS/Na+-MMT and modified PS/Na+-MMT/MMA and PS/Na+-MMT/St nanocomposites were studied with X-ray diffraction (XRD), differential scanning calorimetry (DSC), and TGA, as well as mechanical properties. It was found that the PS/Na+-MMT/St nanocomposites presented better thermal properties and an improvement in Young’s modulus (YM) in compared to PS/Na+-MMT/MMA nanocomposites.

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Publisher

Hindawi Publishing Corporation,Hindawi,John Wiley & Sons, Inc

Subject

Carbon fibers

/ Clay

/ Composite materials

/ Emulsion polymerization

/ Fourier transforms

/ Infrared analysis

/ Investigations