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Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid
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Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid
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Journal Article
Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid
2018
Overview
We synthesized Pd-Fe series nanoparticles in solid solution using pulsed plasma in liquid with Pd-Fe bulk mixture electrodes. The Pd-Fe atomic percent ratios were 1:3, 1:1, and 3:1, and the particle size was measured to be less than 10 nm by high-resolution transmission electron microscopy (HR-TEM). The nanoparticles showed face-centered cubic structure. The lattice parameter increased with increasing Pd content and followed Vegard’s law, and energy-dispersive X-ray spectra were consistent with the ratios of the starting samples, which showed a solid solution state. The solid solution structure and local structure were confirmed by HR-TEM and X-ray absorption fine structure.
Publisher
MDPI AG,MDPI
Subject
