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氨基酸离子液体［bmim］Gly的合成探索及表征
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Journal Article
氨基酸离子液体［bmim］Gly的合成探索及表征
2014
Overview
X51%O626.2; 探索两步法合成1-丁基-3-甲基咪唑甘氨酸离子液体（[ bmim] Gly）的反应条件。第一步，采用阴离子树脂静态交换法由1-丁基-3-甲基咪唑溴盐（[ bmim ] Br ）与强碱性阴离子树脂生成中间产物1-丁基-3-甲基咪唑氢氧化物（[bmim]OH），通过单因素实验获得其最佳交换条件；第二步，[ bmim ] OH 与甘氨酸（ Gly ）反应，经脱水、洗涤后得目标产物。对产物进行核磁（1H NMR）和红外（IR）表征，结果表明产品纯度较高。与动态合成法相比，静态法合成[ bmim] Gly操作简便，节水省时，有助于实现氨基酸离子液体合成过程的绿色化和工业化。
Publisher
南京理工大学 江苏省化工污染控制与资源化高校重点实验室，南京，210094%南京理工大学 江苏省化工污染控制与资源化高校重点实验室，南京，210094,南京信息工程大学 江苏省大气环境监测与污染控制高技术研究重点实验室，南京，210044
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