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Syntheses and proton conductivity of mesoporous Nd.sub.2O.sub.3-SiO.sub.2 and NdOCl-SiO.sub.2 composites
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Syntheses and proton conductivity of mesoporous Nd.sub.2O.sub.3-SiO.sub.2 and NdOCl-SiO.sub.2 composites
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Journal Article
Syntheses and proton conductivity of mesoporous Nd.sub.2O.sub.3-SiO.sub.2 and NdOCl-SiO.sub.2 composites
2012
Overview
Two mesoporous oxide composites of [Nd.sub.2][O.sub.3]Si[O.sub.2] and NdOCl-Si[O.sub.2] were synthesized using SBA-15 as a template and neodymium nitrate or neodymium chloride as a precursor. The porous [Nd.sub.2][O.sub.3]-Si[O.sub.2] with a SBA-15like structure has amorphous walls and the porous NdOCl-Si[O.sub.2] with a replicated structure of SBA-15 has crystalline walls. These porous materials were characterized by X-ray diffraction, transmission electron microscopy and nitrogen adsorption/desorption. They exhibited significant proton conductivities in the presence of moisture at low temperatures and the highest conductivity observed was 4.55 x [10.sup.-4]S/cm at 47°C in wet air (RH = 28.6%).
Publisher
Springer
Subject
