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Rh-Catalyzed Cascade C-H Activation/Annulation of IN/I-Hydroxybenzamides and Propargylic Acetates for Modular Access to Isoquinolones
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Rh-Catalyzed Cascade C-H Activation/Annulation of IN/I-Hydroxybenzamides and Propargylic Acetates for Modular Access to Isoquinolones
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Journal Article
Rh-Catalyzed Cascade C-H Activation/Annulation of IN/I-Hydroxybenzamides and Propargylic Acetates for Modular Access to Isoquinolones
2022
Overview
A sequential Rh(III)-catalyzed C-H activation/annulation of N-hydroxybenzamides with propargylic acetates leading to the formation of NH-free isoquinolones is described. This reaction proceeds through a sequential C-H activation/alkyne insertion/intramolecular annulation/N-O bond cleavage procedure, affording a broad spectrum of products with diverse substituents in moderate-to-excellent yields. Notably, this protocol features the simultaneous formation of two new C-C/C-N bonds and one heterocycle in one pot with the release of water as the sole byproduct.
Publisher
MDPI AG
Subject
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