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Effect of sintering temperature on microstructure and electrical properties of Mn sub(1.2)Co sub(1.5)Ni sub(0.3)O sub(4) ceramic materials using nanoparticles by reverse microemulsion method
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Effect of sintering temperature on microstructure and electrical properties of Mn sub(1.2)Co sub(1.5)Ni sub(0.3)O sub(4) ceramic materials using nanoparticles by reverse microemulsion method
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Effect of sintering temperature on microstructure and electrical properties of Mn sub(1.2)Co sub(1.5)Ni sub(0.3)O sub(4) ceramic materials using nanoparticles by reverse microemulsion method
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Journal Article
Effect of sintering temperature on microstructure and electrical properties of Mn sub(1.2)Co sub(1.5)Ni sub(0.3)O sub(4) ceramic materials using nanoparticles by reverse microemulsion method
2016
Overview
The high performance Mn sub(1.2)Co sub(1.5)Ni sub(0.3)O sub(4) (MCN) ceramic materials are successfully fabricated using nanoparticles which are synthesized by the reverse microemulsion method. The morphology, crystal structure and particle size distribution of MCN nanoparticles are characterized by the XRD, SEM, TEM and HRTEM. The results show the well single tetragonal spinel structure and the narrow particle size distribution about 40 nm. As the sintering temperature increasing from 1000 to 1250 degree C, all the MCN ceramic samples prepared by above-mentioned nanoparticles show the same single tetragonal spinel structure. The thermal sensitive properties with high values of Ie sub(25), B sub(25/100), E sub(a), and alpha sub(25) of MCN ceramics at different sintering temperatures are in the range of 68,805-497,730 Omega cm, 4578-5159 K, 0.395-0.445 eV, and -5.2 to -5.8 %/K, respectively. These features indicate that the microstructure and electrical properties of MCN ceramics are relevant to the sintering temperature.
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