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Synergistic Effect between Piperazine Pyrophosphate and Melamine Polyphosphate in Flame Retardant Coatings for Structural Steel
Piperazine pyrophosphate (PAPP) combined with melamine polyphosphate (MPP) was adopted to prepare a waterborne fire retardant intumescent coating (IC) for structural steel. Silicone acrylic emulsion was used as binder. In the 2-h torch test, PAPP/MPP-IC coating presented excellent fire resistance performance. The equilibrium temperature at the backside of the steel board decreased to 170 °C with protection of MPP/PAPP-IC, compared with 326 °C of APP/PER/MEL-IC. After 72-h water immersion, MPP/PAPP-IC could still provide sufficient thermal isolation, but APP/PER/MEL-IC failed the test. The water absorption of the MPP/PAPP coating was also reduced. The thermogravimetric analysis measured that the PAPP/MPP-IC had unique initial decomposition temperature of 296 °C and higher residue of 33.8 wt%, which demonstrated better thermal stability and fire retardancy in condensed phase. In addition, Scanning Electron Microscope (SEM) images illustrated that the structure of the carbon layer formed by MPP/PAPP-IC was dense, complete and consistent, indicating the improvement of mechanical strength and thermal isolation of the char. The synergistic effect between piperazine and phosphoric acid groups in MPP/PAPP contributed to the superior flame retardancy. Consequently, MPP/PAPP-IC was much more efficient than the traditional APP/PER/MEL-IC. This work provides a novel way for designing flame retardant coatings for structural steel with excellent comprehensive performance.
Journal Article
Advanced steel design of structures
\"Advanced Steel Design of Structures examines the design principles of steel members under special loads and covers special geometric forms and conditions not typically presented in standard design books. It explains advanced concepts in a simple manner using numerous illustrative examples and MATLABھ codes. Features: Provides analysis of members under unsymmetrical bending Includes coverage of structures with special geometry and their use in offshore applications for ultra-deep water oil and gas exploration Presents numerical modeling and analysis of steel members under fire conditions, impact, and blast loads Includes MATLABھ examples that will aid in the capacity building of civil engineering students approaching this complex subject Written for a broad audience, the presentation of design concepts of steel members will be suitable for upper-level undergraduate students. The advanced design theories for offshore structures under special loads will be an attractive feature for post-graduate students and researchers. Practicing engineers will also find the book useful, as it includes numerous solved examples and practical tutorials\"-- Provided by publisher.
Book
On the Heat-Affected Zone Role for Mechanical Properties of Structural-Steel MIG and CMT–MIG Weldments
The effect of evolved heat-affected zone (HAZ) during metal inert gas (MIG) and cold metal transfer (CMT)–MIG welding of two IS2062 structural-steels, i.e. E250 and E410, was studied. The comparison of mechanical properties such as yield strength, ultimate tensile strength, tensile ductility being represented by %elongation, impact toughness at room temperature, and microhardness was done. Conventional optical and field-emission scanning electron microscopy were used for detailed examination of microstructural evolution across weldments. CMT–MIG in comparison to MIG mode was observed to produce a well-refined microstructure for both E250 and E410. Various HAZ subzones comprised of fully formed pearlite colonies in coarse-grain HAZ, pearlite in patched form in fine-grain HAZ, partially distributed pearlite in inter-critical HAZ, and fine Widmanstätten and acicular ferrite in deposited weld-metal of ER-70S6. Such microstructural manifestations particularly in HAZ subzones exhibited a positive effect leading to improved mechanical performance.
Journal Article
Examining Shape Dependence on Small Mild Steel Specimens during Heating Processes
With regard to the heating technology of small test specimens (D < 1 inch, i.e., 25.4 mm), only a limited amount of data and literature are available for making adequate technological decisions. Heating time of small geometric shapes is influenced by the technological parameters of the furnace, the temperature, the disposition technique in the furnace and the geometric characteristics of the workpiece. How to shorten heating time to achieve a suitable material structure is a vital question, while considerable energy is saved at the same time. Among the geometric characteristics, shape dependence is one of the important aspects that must be taken into account in terms of heating technology. Shape dependence is usually taken into account with empirically produced correction factors, which can result in significant oversizing of heating time, energy-wasting technology and material structure of insufficient fineness. In the course of our work, we investigated and compared the shape dependence of cylindrical and prismatic specimens with the same surface-to-volume ratios, which were combined with surface heat transfer analyses and geometric effect tests to formulate new approximate equations for determining heating time. As a result, we could mathematically derive a relationship between heating time, size and shape of the active surfaces, the correlation of which can shorten heating time by 20%. In addition, a shape factor (1.125) between cylinder and prismatic-shaped specimens was determined, which can be used with the new equation to calculate heating time for similar specimens. At last, a relationship is developed between the amount of heat that can be stored in the body during heat equalization and the complexity of the shape, which can be characterized through ratios depending on heating times and active surfaces in the function of total surface/volume ratio. Based on this relationship it can be determined more precisely when heat equalization occurs; therefore, shorter heating time can be achieved. In conclusion, with the help of this new method, optimal heating time for structural steel components, in the case of small cross-section and weight, can be determined.
Journal Article
Assessment of Selected Structural Properties of High-Speed Friction Welded Joints Made of Unalloyed Structural Steel
Commonly used S235JR structural steel, generally associated with good weldability, was joined by high-speed friction welding (HSFW). The friction welding tests were performed with a rotational speed of n = 8000 rpm and four different values of the unit pressure in the friction phase (pf) in the range of 64–255 MPa. The obtained joints were subjected to metallographic observations using an optical microscope; in selected zones of friction joints the average grain size was specified in accordance with the EN ISO 643:2012 standard; the hardness of friction joints was measured using the Vickers method. The friction-welded joint with the highest pf was EBSD-investigated. The obtained friction-welded joints resembled an hourglass, and the microstructure of individual zones of the joints differed depending on the height (axis, radius) of the observations. The generated joining conditions resulted in a significant refinement of the microstructure in the friction weld—the average grain size is about 1 µm2 (for base material it was 21 µm2). The highest increase in hardness above 340 HV0.1 was recorded in the friction weld of the welded joint with the lowest used value pressure in the friction phase. Such a sharp increase in hardness can make the resulting friction-welded joint become sensitive to dynamic or fatigue loads. The electron backscatter diffraction (EBSD) investigation confirmed the strong refinement of the microstructure in the friction-welded joint and the occurrence of the phenomenon of dynamic recrystallization (DRX). The friction weld was also characterized by a large share of high-angle boundaries (HAGBs) >80%. These results may indicate that during high-speed friction welding it is possible to create conditions like those obtained during the High-Pressure Torsion (the method used to produce UFG materials) process.
Journal Article
Approach for the Static Design of Arc-Brazed Fillet Welds from CuAl7 on Low-Alloyed Constructional Steel
This publication covers experimental investigations on the design resistance of arc-brazed fillet welds (CuAl7) on low-alloyed structural steel (S355) subject to predominantly static loading and regarding steel construction regulations (Eurocode). In current steel construction regulations, there is no standardized design approach for arc-brazed fillet welds available, so arc-brazed connections are rarely used despite the benefits they offer in several regards compared to conventionally welded connections. Therefore, a resistance model for arc-brazed fillet welds was calibrated based on tensile tests that were conducted on gas metal arc-brazed specimens with transverse and longitudinal fillet welds. Based on the statistical evaluation of the test results according to Annex D of EN 1990, a newly determined correlation factor βb is proposed, which can be used for the static design of arc-brazed fillet welds made of CuAl7. This approach leads to a significantly higher calculated design resistance than previous non-standardized design approaches allowed. Also, it was found that the failure behavior of the fillet welds is critical for the design resistance of the joints and that there is a need for further investigations with regard to a targeted joint failure, which, analogous to welded fillet welds, should take place along the throat of the weld and not along the less resistant diffusion zone of the joint. Thus, the results underscore the potential for the use of arc-brazed connections in steel construction in regard to their load-bearing capacity, but also highlight the necessity of continued research regarding factors influencing their structural integrity.
Journal Article