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One-step synthesis of highly reactive g-C3N4
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One-step synthesis of highly reactive g-C3N4
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Journal Article
One-step synthesis of highly reactive g-C3N4
2022
Overview
Graphitic carbon nitride (g-C
3
N
4
) with well-controlled properties are the key for photocatalysis water splitting and organic pollutant degradation. A facile template-free synthesis method was utilized to optimize the polymerization temperature of melamine and urea for the preparation of highly active g-C
3
N
4
. The polymerization was carried out at different temperatures and ramping rate in tightly sealed crucible system with open air conditions. The crystalline and tri-s-triazine periodicity was significantly improved with increasing polymerization temperature. The results demonstrated that graphitic carbon nitride could not be fully formed below 550 °C. It was also found that the precursors and heating rate had a big influence on the photocatalytic activities. Higher photocatalytic activities were achieved by g-C
3
N
4
synthesized from urea at a lower heating rate.
Publisher
Springer US,Springer Nature B.V
