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Mechanochemical Synthesis of a Cocrystal of Two Supramolecular Hydrogen-Bonded Aggregates of 1,3,6,8-Tetraazatricyclo4.3.1.13,8undecane (TATU) with 4-tert-Butylphenol Bearing Different Hydrogen Bonding Interactions
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Mechanochemical Synthesis of a Cocrystal of Two Supramolecular Hydrogen-Bonded Aggregates of 1,3,6,8-Tetraazatricyclo4.3.1.13,8undecane (TATU) with 4-tert-Butylphenol Bearing Different Hydrogen Bonding Interactions
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Mechanochemical Synthesis of a Cocrystal of Two Supramolecular Hydrogen-Bonded Aggregates of 1,3,6,8-Tetraazatricyclo4.3.1.13,8undecane (TATU) with 4-tert-Butylphenol Bearing Different Hydrogen Bonding Interactions
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Journal Article
Mechanochemical Synthesis of a Cocrystal of Two Supramolecular Hydrogen-Bonded Aggregates of 1,3,6,8-Tetraazatricyclo4.3.1.13,8undecane (TATU) with 4-tert-Butylphenol Bearing Different Hydrogen Bonding Interactions
2018
Overview
The synthesis and single crystal structure of a new cocrystal, which is composed of OHphenolic∙∙∙OHphenolic∙∙∙Naminalic supramolecular heterosynthons assembled from 4-tert-butylphenol and the macrocyclic aminal TATU, is presented. This cocrystal was prepared by solvent-free assisted grinding, which is a commonly used mechanochemical method. Crystal structure, supramolecular assembly through hydrogen bonding interactions as well as the physical and spectroscopic properties of the title cocrystal are presented in this paper.
Publisher
MDPI AG
