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Novel Glucosylimidazolium Ionic‐Liquid‐Supported Novozym 435 Catalysts – A Proof of Concept for an Acrylation Reaction
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Novel Glucosylimidazolium Ionic‐Liquid‐Supported Novozym 435 Catalysts – A Proof of Concept for an Acrylation Reaction
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Novel Glucosylimidazolium Ionic‐Liquid‐Supported Novozym 435 Catalysts – A Proof of Concept for an Acrylation Reaction
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Journal Article
Novel Glucosylimidazolium Ionic‐Liquid‐Supported Novozym 435 Catalysts – A Proof of Concept for an Acrylation Reaction
2022
Overview
A series of novel ionic liquids based on glucose was synthesized in high yields in simple two or three‐step reaction procedures. These carbohydrate‐based ionic liquids were studied and compared to commercially available imidazolium‐based ionic liquids as supports for Novozym 435 in the acrylation of n‐butanol. A direct correlation between the availability of hydroxy groups and the overall activity as well as an enhanced recyclability of the biocatalyst has been found for the glucose‐based ionic liquids.
Biocatalysis, given its mild reaction conditions, is an important tool for the construction of acrylic esters, monomer assets in chemical industry, which are usually unstable against acids and heat. Several examples of ionic liquids were tested as supports for Novozym 435 in the construction of butyl acrylate Both a higher yield and a stable recyclability were found for the herein‐reported glucosylimidazolium‐based ionic liquids.
