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$Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD$

Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD

by Bromley, Dan , Branford, Will R , Carter-Gartside, Jack N , Och, Mauro , Haigh, Sarah , Tillotson, Evan , Vanstone, Alex , Mattevi, Cecilia , Eggeman, Alexander , Heutz, Sandrine , Navarro-Moratalla, Efrén , Rimmer, Max , Deng, Siyuan , Maity, Indrajit , Kho Zhiquan , Sullivan-Allsop, Sam , Mione, Filippo , Parker, Joseph , Tainton, Gareth R M , Cai, Rongsheng , Lischner, Johannes C , Tanwar, Khagesh , Duran, Ercin C , Bai, Haoyu

in Chemical synthesis / Crystal growth / Electron diffraction / Ferromagnetism / Low temperature / Magnetic properties / Magnets / Metalorganic chemical vapor deposition / Organic chemicals / Organic chemistry / Perturbation theory / Raman spectroscopy / Spintronics

2025

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Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD

2025

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$Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD$

Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD

2025

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$Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD$

Paper

Phase engineering of 1T\$'\$ and 1T CrS2 and Cr2S3 by MOCVD

Bromley, Dan,

Branford, Will R,

Carter-Gartside, Jack N,

Och, Mauro,

Haigh, Sarah,

Tillotson, Evan,

Vanstone, Alex,

Mattevi, Cecilia,

Eggeman, Alexander,

Heutz, Sandrine,

Navarro-Moratalla, Efrén,

Rimmer, Max,

Deng, Siyuan,

Maity, Indrajit,

Kho Zhiquan,

Sullivan-Allsop, Sam,

Mione, Filippo,

Parker, Joseph,

Tainton, Gareth R M,

Cai, Rongsheng,

Lischner, Johannes C,

Tanwar, Khagesh,

Duran, Ercin C,

Bai, Haoyu

2025

Overview

Layered Cr-chalcogenides compounds offer a rich range of crystal phases with different magnetic properties some of which have been predicted only but not experimentally verified. Here we demonstrate a previously unreported crystal phase of CrS2, namely the distorted octahedral (1T\$'\$) structure, synthesized via metal-organic chemical vapour deposition (MOCVD). We achieved the tuneable synthesis of either 1T\$'\$ or 1T phase CrS2. The structure were identified using polarized Raman spectroscopy, density functional perturbation theory (DFPT), as well as scanning electron diffraction (4D-STEM). 4D-STEM reveals that 1T\$'\$ crystals grow from an originally nucleated kinetically favoured 1T phase which then transform into the thermodynamically stable 1T\$'\$ phase. Magneto-optic Kerr imaging reveals that the 1T\$'\$ CrS2 crystals have soft ferromagnetic nature at low temperature. Our MOCVD growth of complex phases of 2D CrS2 with long-range magnetic order paves the way for the scalable synthesis of 2D magnets for ultrathin magnetic memories for logic-in-memory applications and spintronics.

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Publisher

Cornell University Library, arXiv.org

Subject

Chemical synthesis

/ Crystal growth

/ Electron diffraction

/ Ferromagnetism

/ Low temperature

/ Magnetic properties

/ Magnets