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Sub-30 nm Fe sub(3)O sub(4) and gamma -Fe sub(2)O sub(3) octahedral particles: preparation and microwave absorption properties
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Sub-30 nm Fe sub(3)O sub(4) and gamma -Fe sub(2)O sub(3) octahedral particles: preparation and microwave absorption properties
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Journal Article
Sub-30 nm Fe sub(3)O sub(4) and gamma -Fe sub(2)O sub(3) octahedral particles: preparation and microwave absorption properties
2013
Overview
A simple low-cost hydrothermal method has been developed to fabricate uniformly dispersed octahedral Fe sub(3)O sub(4) nanoparticles with tunable size. The particle size can be reduced to 20-30 nm under the effect of phosphate, meanwhile, the edetate disodium can improve the dispersivity of particles. High-resolution transmission electron microscope showed that the octahedral Fe sub(3)O sub(4) nanoparticle was enclosed by eight (111) planes. Octahedral gamma -Fe sub(2)O sub(3) nanoparticles were obtained by reoxidizing the as-synthesized Fe sub(3)O sub(4) nanoparticles. The microwave absorption properties of the octahedral Fe sub(3)O sub(4) and gamma -Fe sub(2)O sub(3) nanoparticles were measured in the frequency range of 2-18 GHz. A minimum reflection loss of -28 dB was observed at 8.6 GHz for octahedral Fe sub(3)O sub(4) nanoparticles.
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