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Fabrication of potato-like silver molybdate microstructures for photocatalytic degradation of chronic toxicity ciprofloxacin and highly selective electrochemical detection of H2O2
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Fabrication of potato-like silver molybdate microstructures for photocatalytic degradation of chronic toxicity ciprofloxacin and highly selective electrochemical detection of H2O2
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Fabrication of potato-like silver molybdate microstructures for photocatalytic degradation of chronic toxicity ciprofloxacin and highly selective electrochemical detection of H2O2
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Journal Article
Fabrication of potato-like silver molybdate microstructures for photocatalytic degradation of chronic toxicity ciprofloxacin and highly selective electrochemical detection of H2O2
2016
Overview
In the present work, potato-like silver molybdate (Ag
2
MoO
4
) microstructures were synthesized through a simple hydrothermal method. The microstructures of Ag
2
MoO
4
were characterized by various analytical and spectroscopic techniques such as XRD, FTIR, Raman, SEM, EDX and XPS. Interestingly, the as-prepared Ag
2
MoO
4
showed excellent photocatalytic and electrocatalytic activity for the degradation of ciprofloxacin (CIP) and electrochemical detection of hydrogen peroxide (H
2
O
2
), respectively. The ultraviolet-visible (UV-Vis) spectroscopy results revealed that the potato-like Ag
2
MoO
4
microstructures could offer a high photocatalytic activity towards the degradation of CIP under UV-light illumination, leads to rapid degradation within 40 min with a degradation rate of above 98%. In addition, the cyclic voltammetry (CV) and amperometry studies were realized that the electrochemical performance of Ag
2
MoO
4
modified electrode toward H
2
O
2
detection. Our H
2
O
2
sensor shows a wide linear range and lower detection limit of 0.04–240 μM and 0.03 μM, respectively. The Ag
2
MoO
4
modified electrode exhibits a high selectivity towards the detection of H
2
O
2
in the presence of different biological interferences. These results suggested that the development of potato-like Ag
2
MoO
4
microstructure could be an efficient photocatalyst as well as electrocatalyst in the potential application of environmental, biomedical and pharmaceutical samples.
Publisher
Nature Publishing Group UK,Nature Publishing Group
Subject
