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In Situ Fabrication of Electrospun Carbon Nanofibers–Binary Metal Sulfides as Freestanding Electrode for Electrocatalytic Water Splitting
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In Situ Fabrication of Electrospun Carbon Nanofibers–Binary Metal Sulfides as Freestanding Electrode for Electrocatalytic Water Splitting
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Journal Article
In Situ Fabrication of Electrospun Carbon Nanofibers–Binary Metal Sulfides as Freestanding Electrode for Electrocatalytic Water Splitting
2021
Overview
In search of effective and stable bifunctional electrocatalyst for electrocatalytic water splitting is still a major challenge for the highly efficient H
2
production. Here, we reported a facile strategy to design high-indexed Cu
3
Pd
13
S
7
nanoparticles (NPs) in situ synthesized on the three-dimensional (3D) carbon nanofibers (CNFs) by combining electrospinning and chemical vapor deposition (CVD) technology. The high-index facets with abundant active sites, the 3D architecture CNFs with high specific surface area and synergistic effect of Cu–Pd–S bonds with strong electron couplings together promote the electrocatalytic performance. The Cu
3
Pd
13
S
7
/CNFs shows excellent electrocatalytic activity with low overpotentials of 52 mV (10 mA cm
−2
) for hydrogen evolution reaction (HER) and 240 mV (10 mA cm
−2
) for oxygen evolution reaction (OER). The excellent protection of Cu
3
Pd
13
S
7
by CNFs from aggregation and electrolyte corrosion lead to the high stability of Cu
3
Pd
13
S
7
/CNFs under acidic and alkaline conditions.
Publisher
Springer Singapore,Springer Nature B.V
