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High-Resolution EM of Colloidal Nanocrystal Growth Using Graphene Liquid Cells

by Crommie, Michael F. , Park, Jungwon , Zettl, A. , Ercius, Peter , Alivisatos, A. Paul , Hellebusch, Daniel J. , Lee, Jeong Yong , Yuk, Jong Min , Kim, Kwanpyo

in Cell growth / Coalescence / Coalescing / Colloids / Crystal twinning / Crystals / Electron, positron and ion microscopes, electron diffractometers and related techniques / Entrapment / Evaporation / Exact sciences and technology / Fees / Fundamental areas of phenomenology (including applications) / Graphene / image analysis / Image forming and processing / Imaging / Imaging and optical processing / Instruments, apparatus, components and techniques common to several branches of physics and astronomy / Liquids / Monomers / Nanocrystals / Nanoparticles / Nanotechnology / Optics / Physics / Platinum / Silicon / transmission electron microscopy

2012

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High-Resolution EM of Colloidal Nanocrystal Growth Using Graphene Liquid Cells

by Crommie, Michael F. , Park, Jungwon , Zettl, A. , Ercius, Peter , Alivisatos, A. Paul , Hellebusch, Daniel J. , Lee, Jeong Yong , Yuk, Jong Min , Kim, Kwanpyo

2012

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High-Resolution EM of Colloidal Nanocrystal Growth Using Graphene Liquid Cells

by Crommie, Michael F. , Park, Jungwon , Zettl, A. , Ercius, Peter , Alivisatos, A. Paul , Hellebusch, Daniel J. , Lee, Jeong Yong , Yuk, Jong Min , Kim, Kwanpyo

2012

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Journal Article

High-Resolution EM of Colloidal Nanocrystal Growth Using Graphene Liquid Cells

Crommie, Michael F.,

Park, Jungwon,

Zettl, A.,

Ercius, Peter,

Alivisatos, A. Paul,

Hellebusch, Daniel J.,

Lee, Jeong Yong,

Yuk, Jong Min,

Kim, Kwanpyo

2012

Overview

We introduce a new type of liquid cell for in situ transmission electron microscopy (TEM) based on entrapment of a liquid film between layers of graphene. The graphene liquid cell facilitates atomic-level resolution imaging while sustaining the most realistic liquid conditions achievable under electron-beam radiation. We employ this cell to explore the mechanism of colloidal platinum nanocrystal growth. Direct atomic-resolution imaging allows us to visualize critical steps in the process, including site-selective coalescence, structural reshaping after coalescence, and surface faceting.

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Publisher

American Association for the Advancement of Science,The American Association for the Advancement of Science

Subject

/ Electron, positron and ion microscopes, electron diffractometers and related techniques