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Coating of structured catalytic reactors by plasma assisted polymerization of tetramethyldisiloxane
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Coating of structured catalytic reactors by plasma assisted polymerization of tetramethyldisiloxane
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Journal Article
Coating of structured catalytic reactors by plasma assisted polymerization of tetramethyldisiloxane
2011
Overview
An original process based on cold plasma assisted polymerization of tetramethyldisiloxane (TMDSO) in the presence of O2 was developed to cover substrates showing various shapes (plate and foam). In the frame of catalytic application, this coating has to act as a bonding layer for the deposition of active phase such as VOx/TiO2 well‐known for its properties in NOx and volatile organic compounds abatement and in the production of chemical intermediates. Good results were obtained by the deposition of a 5‐μm thick polysiloxane film followed by a thermal treatment under air at 650°C and by a remote nitrogen plasma post treatment. This procedure led to a silica‐like layer allowing its coating in an aqueous suspension of TiO2. Such a multilayered material can be obtained homogeneously on the whole surface of a sample showing a 3D open geometry like metallic foam. Characterizations of the different steps of the elaborated multilayer material were performed by Fourier transformed infrared spectroscopy, Raman spectrometry, X‐ray photoelectron spectroscopy, and electron probe micro‐analyzer. POLYM. ENG. SCI., 2011. © 2011 Society of Plastics Engineers
Publisher
Wiley Subscription Services, Inc., A Wiley Company,Wiley,Society of Plastics Engineers, Inc,Blackwell Publishing Ltd,Wiley-Blackwell
